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,•: -~ <br />Work Order: 07-4617 <br />Client Project ID: Last Chance <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 13180 <br />Sample ID: LCS-13180 SampType: LCS TestCode: TCLPMETAL Run ID: ICP-OPTIMA 5300 DV_070801A Prep Date: 8/1/07 Units: mg/L <br /> Batch ID: 13180 TestNo: SW1311/6010 FileID: 080107PM Analysis Date: 8/1/07 SegNo: 590935 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Barium 27.47 2.0 25 0.0004158 110 75 125 0 0 <br />Cadmium 1.029 0.10 1 0.0008566 103 82.11 109.37 0 0 <br />Chromium 10.54 0.50 10 •0.0005539 105 80 120 0 0 <br />Lead 10.74 0.50 10 0.006229 107 79.35 108.06 0 0 <br />Selenium 10.36 0.50 10 -0.01281 104 68.13 115.93 0 0 <br />Silver 0.9969 0.050 1 -0.0007757 99.7 59.18 127.15 0 0 <br />Sample ID: 07-4958-01AMS SampType: MS TestCode: TCLPMETAL Run ID: ICP-OPTIMA 5300 DV_070801A Prep Date: 8/1/07 Units: mg/L <br /> Batch ID: 13180 TestNo: SW1311/6010 FileID: 080107PM Analysis Date: 8/1/07 SegNo: 590943 <br />Analyte Result LOL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Arsenic 0.9237 0.50 1 0 92.4 50 150 0 0 <br />Barium 8.711 2.0 5 4.015- 93.9 50 150 0 0 <br />Cadmium 0.4716 0.10 0.5 0 94.3 50 150 0 0 <br />Chromium 4.625 0.50 5 0 92.5 50 150 0 0 <br />Lead 1.985 0.50 2 0 99.2 50 150 0 0 <br />Selenium 2.806 0.50 3 0 93.5 50 150 0 0 <br />Silver 0.3958 0.050 0.5 0 79.2 50 150 0 0 <br />Sample ID: 07-4700-01AMS SampType: MS TestCode: TCLPMETAL Run ID: ICP-OPTIMA 5300 DV_070801A Prep Date: 8/1/07 ,Units: mg/L <br /> Batch ID: 13180 TestNo: SW131116010 FileID: 080107PM Analysis Date: 8/1/07 SegNo: 590950 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Arsenic <br />Barium <br />Cadmium <br />Chromium <br />Lead <br />Selenium <br />Silver <br />0.6893 0.50 <br />7.137 2.0 <br />0.4706 0.10 <br />4.646 0.50 <br />1.972 0.50 <br />3.013 0.50 <br />0.3579 0.050 <br />1 0 68.9 50 <br />5 2.362 95.5 50 <br />0.5 0 94.1 50 <br />5 0 92.9 50 <br />2 0 98.6 50 <br />3 0 100 50 <br />0.5 0 71.6 50 <br />150 0 0 <br />150 0 0 <br />150 0 0 <br />150 0 0 <br />150 0 0 <br />150 0 0 <br />150 0 0 <br />Qualifiers: U -Not detected at or above the Reporting Limit R -RPD outside acceptance limits <br />J -Analyte detected below quantitation limits B -Analyte detected in the associated Method Blank <br />S -Spike Recovery outside acceptance limits H -Prep or analytical holding time exceeded <br />E -Extrapolated value, value exceeds calibration range. X -See case narrative <br />