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work order: o~-46I~ ANALYTICAL QC SUMMARY REPORT <br />Client Project ID: Last Chance <br />BatchID: 13180 <br />Sample ID: MB-13180/13115 SampType: MBLK TestCode: TCLPMETAL Run ID: ICP-OPTIMA 5300 DV_070801A Prep Date: 8/1/07 Units: mg/L <br /> Batch ID: 13180 TestNo: SW1311/6010 FileID: 080107PM Analysis Date: 8/1/07 SegNo: 590944 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Silver 0 0.050 <br />Uranium 0 0 <br />Vanadium 0 0 <br />Zinc 0.5044 0.10 <br />Sample ID: MB-13180/13163 SampType: MBLK TestCode: TCLPMETAL Run ID: ICP-OPTIMA 5300 DV_070801A Prep Date: 8/1/07 Units: mg/L <br /> Batch ID: 13180 TestNo: SW1311/6010 FileID: 080107PM Analysis Date: 8/1/07 SegNo: 590972 <br />Analyte Result LOL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Aluminum 0 0.11 <br />Arsenic 0 0.50 <br />Barium - 0 2.0 <br />Cadmium 0 0.10 <br />Chromium 0 0.50 <br />Copper 0 0.025 <br />Iron 0 0.35 <br />Lead 0 0.50 <br />Molybdenum 0 0.025 <br />Nickel 0 0.010 <br />Selenium 0 0.50 <br />Silver 0 0.050 <br />Uranium 0 0 <br />Vanadium 0 0 <br />Zinc 0 0.10 <br />Sample ID: LCS-13180 SampType: LCS TestCode: TCLPMETAL Run ID: ICP-OPTIMA 5300 DV_070801A Prep Date: 8/1/07 Units: mg/L <br /> Batch ID: 13180 TestNo: SW1311/6010 FileID: 080107PM Analysis Date: 8/1/07 SegNo: 590935 <br />Analyte Result LOL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Arsenic 10,02 0.50 10 0.02995 100 71.04 124.4 0 0 <br />Qualifiers: U -Not detected at or above the Reporting Limit R -RPD outside acceptance limits <br />J -Analyte detected below quantitation limits B -Analyte detected in the associated Method Blank <br />S -Spike. Recovery outside acceptance limits H -Prep or analytical holding time exceeded <br />E -Extrapolated value, value exceeds calibration range. X -See case narrative <br />