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A i C 1 <br />v • .• M.'• M1 •~~,r„ n • ~ Lid <br />~YYa/YL• <br />6ample bottles should ba comptetaly furl. to the point of ovorfbwlnp, such that tllara k no <br />drspaca in tM ample. 8rmplu should M atorad and ahlppad In the daR n a tampmtun <br />of rata ttun a Oepnae cantlptada. <br />TM ample ai>ti u wtticlant to .pow npGatirM a total cyanid. daprmtnatbna by the <br />manual method when accurfoy at wry kw aotwantnttona tl.e. 0.06 mOA. a Iasi b <br />/squired. <br />3,1,4 Lyalmatar l1 amplq <br />Lyaimater samptea praant particular sampllnp and analytical problama. Lyalmaten, shad M <br />unsatunUd madla adlacant to mine wasp ficalttes, rarely produce auHiclani water for <br />wbsuntlva and manlnpful ohamical anNysh 6a to done, unlea iharo 1^ vpluminaya Wtuga <br />from the wanr f~clllty. <br />FvRhumon, h k nct poaalbla to purpa the ry^Imaer to rid the It of particulates matiri.i, <br />praipitaps er nenaqulllbrlum (laid, ss la both normal and mandated for a monimdnp wall, <br />as there la so Ilttla HmDb and tM lyalmater would nm^in cry aher the inltid purplnp. <br />Aceordtnply, any aefid partlelas In tM tysimatar, Inciudinp aub•O,ab micron ebya and <br />colloids, wIN ba antratnad In the smell ample volume and nn hwa the potential to affect <br />tree eysn(ea analysis, fsa action 3.a 6adow). <br />In the case of lyalmapr L3, the throe s^mpla^ oollacpd wen 720 mlc, 20 m!a and 8 ml~. <br />Consaovantiy, all pMlculaus from tM ryelmstars would ba eoncanvated In tress small <br />volumes of fluid, as ODpoaed to hetnp flusnod from the sampllnp aystam and the raaldusl <br />dlaparsed In ens litres of fluid a would ba the nauh from norm^I samDlinp protocol. <br />3.Z Praaavatlon tachnigw <br />3.1.1 StenderC c~tarvetlor. pro:oco <br />!n crdo+ :D Ory vtnt fret cv^r.~tr ,c~< ICN~) !rc-. 1ur',~^[ ny Gr[Y^ [it n;0• snt ~pql. [ n; <br />hpr+' •r.a ^:d!:J rl^~[ a arc t`,ra[. !flan' ~ ;'., rr'~; h cy't' ;.' c_': t/:rr ;IC'~. Va is°p a <br />p" ,E~•J~ I[ k[p: eDOH G^. t i, ,+~`Lr[ nyG rL~af. q'erd tt ,viii not ba pr.r ar.:. SereD~^ DM q <br />torr^ctad t0 ahOve pH 11 by ua1~0 tod~~m or ppln [vm hyproaides. 4nhar cf th^cY <br />pnaernt'ron raspenta era normally added Ctrattly :C :hc amber place tamplinp Ccttla py trees <br />malytlnl iabontorv which tuppiica the sampllnp bonlU to tM templ0 cDl4ctor. <br />Conaaquenay, the torratt smouct e! fret pRSe+v1:~~~~ rta~Mi }Cr Dns litre D! Tu10 le aCd[C <br />tc tM ampry tetyas. an~minp tht: tnay will by f,:;ed co^Glrely w{in ffwd. <br />