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~ • - <br />A f C 1 <br />M wmmary , the tpnl cyanide tan entl antr teNwM attandaM noUti0n to iM date by <br />Aecudaba, to as folbwl: <br />• ampp 12/1E/811 total oyanlda 0.016 tnplli'flote: pw to pmltad wmpla, Inamat OA <br />was not run.• <br />' ample 02/21182: topl ewanlda O.Ot0 «plL; •8ampk 1 8.7W221) evp etealvad Ram <br />holding time for tryanlda aMlyall.' <br />• Nmpla 04/0,7182: tool oyanbe 0.01 t mpA. muddied 4vr to 0.006 mp/L. (ABCI noa: h <br />ahou4d ba noted that ne IrttamalOA could ba run on this /ample, dw to the amad ample <br />e5:a1. <br />~. TECHNICAL ISSl7E4 AfFlCTING DATA VAUDRY <br />7ha follovvlnp Uehnleal laewa, ernonp otneri, haw the poundal of affaednp the wtitllty of <br />the toUl Cyenlde anNyue performed on N• Bmlud volume Of the aampNa CogeCtetl lrom <br />Fytlmanr t 1; <br />• 1. temple else; <br />• 2. proserva6on teehnlqur, <br />' ~• abaenCO Of fltttetioh Ot iampte; <br />' 4. enefyt1O11 method; <br />• 6. absence o! qualhy aewrmn of anatytee; and <br />• d. ebeenca of estimation of the pnctlat qumtlutlon <br />limit, (PCL1, 01 a metho0 tlenetlon Amlt study (M9L1 of the analyses a applletl to thaw <br />typU Of nmplu, <br />To a certain extent, come of that isWO ue Inurllnked an4 then will be a modicum of <br />Overlap in th0 1O110winp tliaCUafiOn of itch M Na tachnfcd Issues, <br />3.1 S^mola S!ae <br />3.1.1 ScendaG aan•p ,r, , c,au fOr enni;e <br />Standard sample protoco~ for cyanlQa darormina4ona In a;uwua media Invplvoe the <br />coUcct:on o< a one litre temple in an ember pleas bon4, Mid et a pH value of anater than <br />pH 12 end tleterminad a soon a poulble, bui within fourteen days ma::mum of umplfnp. <br />To thle and ^nalydcal IeDOretarlea Orovlda ~ottla eonUlnmp the epproprlate amount of <br />preaervetlon agent, venally a~a tp eight pai~•u of sodium hydroxide, for ane ftre of sample. <br />Y <br /> <br />