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Letter/Ann Maest/12-31-93 <br />H. Posey <br />Paget <br />4. I note with interest that the pH of well M-13 had been <br />consistently decreasing over the past year. The Division will ask <br />BMRI about this observation and try to determine why this may be <br />occurring. If the variation is a seasonal trend, and the decrease <br />is an apparent artifact of having only a partial year's worth of <br />sampling and analysis, there will be no further inquiry. if not, <br />we will evaluate the situation further. <br />5. Page 9, first full paragraph states, in part: "Dilution of the <br />sample prior to adding the spike would have resulted in a more <br />reliable spike recovery value." <br />It seems to me, if I understand the situation correctly, that the <br />problem arose not because of the sequence during which the sample <br />was diluted, but rather in the amount of the diluant. It might be <br />more appropriate to word this suggestion more in line with the way <br />it is worded in the conclusion section. The conclusrions section <br />seems more consistent with my understading of the situation. <br />6. Page 9, second full paragraph, refers in part to sevexal pieces of <br />data that were,mis-reported by the laboratory, and a subsequent <br />phone conversation which apparently cleared up the reporting <br />error. <br />There is nothing in the appended documents that would lead a <br />reviewer, independantly, to draw the conclusion reached through <br />the phone conversation. Also, it is certainly poor lab practice <br />to correct results by phone. Therefore, RCG/HBI should procure a <br />letter of explanation along with physical information from Core <br />labs regarding this set of analyses, which will document Core <br />Labs' assessment. Without that information, the lab should re- <br />analyze either these samples or new samples from these collection <br />points. <br />Overall, I am alarmed by the number of paper and analytical mistakes <br />made by Core Labs on this particular set of analyses. If you feel that <br />my alarm is undue, please let me know. However, if you agree, I think <br />it would be appropriate to recommend measures to correct the problem. <br />Another sampling trip may be appropriate, use of another lab may be <br />appropriate, or you may have other recommendations. <br />