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ACZ Laboratories, Inc. <br />2773 Downhill Dnve Steamboat Springs, CO 80487!800) 334-5493 <br />Metals Analysis <br /> ~ r .~ ~. <br />Arsenic, total M200.81CP-MS U mg/L 0.0005 0.003 09116/04 14:13 scp <br />Baron, total M200.7 ICP 0.04 B mg/L 0.01 0.05 09/09104 15:39 wtg <br />Cadmium, total M200.7 ICP U mg/L 0.005 0.02 09/14/04 16:43 wfg <br />Catcrum, dissolved M200.71CP 19.3 mg/L 0.2 1 09!09/04 19:40 wfg <br />Chromium, total M200.7 ICP U mglL 0.01 0.05 09109/04 15:39 wfg <br />Chromium, Tdvalent Calcula0on (Total -Hexavalent) U mglL 0.01 0.05 09121104 15:09 talc <br />Copper, total M200.7 ICP U mglL 0.01 0.05 09109104 15:39 wfg <br />Iron, dissolved M200.71CP 0.02 B mg/1 0.01 0.05 09/09/04 19:40 wig <br />Iron, total M200.71CP 0.43 mg/L 0.01 0.05 09/09104 15:39 wfg <br />Lead, total M200.8 ICP-MS 0.0004 B mg/L 0.0001 0.0005 09176/04 14:13 scp <br />Magnesium, dissolvetl M200,7 ICP 3.4 mg/L 0.2 1 09109/04 19:40 wlg <br />Manganese, dissolved M200.7 ICP U mg/L 0.005 0.03 09/09104 19:40 wfg <br />Manganese, total M200.7 ICP 0.024 B mg/L 0.005 0.03 09109104 15:39 wrg <br />Mercury, total M245.1 CVAA U mglL 0.0002 0.001 09113104 10:42 ak <br />Nickel, total M200.7 ICP U mglL 0.01 0.05 09/09104 15:39 v/fg <br />Selenium, total SM 3114 B, AA-Hydride U mglL 0.001 0.005 09117/04 11:54 jjc <br />Silver, total M200.8 ICP-MS U mglL SE-OS 0.0003 09117/04 19:26 scp <br />Zinc, total M200.7 ICP U mg/L 0.01 0.05 09/09104 15:39 wrg <br />Metals Prep <br />w • r •~ r. <br />Total Hol Plate M200.2 ICP 09/08/04 10:49 ak <br />Digestion <br />Total Hol Plate M200.2 ICP-MS 09108104 8:52 scplgjl <br />Digestion <br />Wet Chemistry <br /> ~ •• r. <br />Chloride M325.2 - Colodmetdc 3 B mglL 1 5 09/08/04 18:39 jr <br />Chromium, Hexavalent SM35000r-D U mglL 0.005 0.03 08126104 13:15 mah <br />Cyanide, total M335.4 - Colorimetric wl distillation U mglL 0.07 0.05 08131/04 15:52 ccp <br />Hardness as CaC03 SM2340B -Calculation 62 mg/L 1 7 09/21/04 15:09 talc <br />Lab Filtration SM 3030 B 08/26/04 13:10 mah <br />Lab Filtration & SM 3030 B 08/31/04 17:30 ak I <br />Acidification <br />Nifrate as N, dissolved Calculation: N03N02 minus N02 0.22 mg/L 0.02 0.7 09/27/04 15:09 talc <br />NilralelNitrile as N, M353.2 -Automated Cadmium 0.22 mglL 0.02 0.1 08/27104 0:20 jr <br /> <br />dissolved <br />Reduction I <br />Nitrite as N, dissolved M353.2 -Automated Cadmium U mg/L O.Ot 0.05 08/27104 0:20 jr <br /> Reduction <br />Nitrogen, ammonia M350.1 -Automated Phenate U mg/L 0.05 0.5 09/16/04 21:47 jr <br /> <br />pH (lab) <br />M150.1 - Eleclrometdc <br />8.3 <br />H <br />units <br />0.1 <br />0.1 <br />08!30/04 12:52 I <br />mah <br />Residue, Filterable M160.1 -Gravimetric 150 mglL 10 20 08131104 18:58 ct <br />(TDS) @780C <br />Sulfate M375.3 -Gravimetric 20 B mg/L 10 50 09/09/04 9:25 jah <br /> <br />Sulfide a5 S <br />M376.2 -Methylene Blue <br />U <br />mg/L <br />0.02 <br />0.1 <br />09/01/04 14:24 I <br />mah <br />REPIN.01.11.00.01 'Please re/er to Extended Qualifier Repoli /or detail <br />Bear Coal Company ACZ Sample ID: L47426.02 <br />Project ID: Date Sampled: 08/25/04 14:00 <br />Sample ID: N.F. GUNNISON-LOWER Date Received: 08/26/04 <br />Sample Matrix: Surface Water <br />