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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487!800) 334-5493 <br />Metals Analysis <br /> • • r •• r. - <br />Arsenic, total M200.8 ICP-MS 0.0006 B mg/L 0.0005 0.003 09116/04 14:08 scp <br />Boron, total M200.7 ICP 0.02 8 mg/L 0.01 0.05 09/09/04 15:36 wfg <br />Cadmium, total M200.7 ICP U mglL 0.005 0.02 09/14104 16:40 wfg <br />Calcium, dissolved M200.7 ICP 20.6 mglL 02 1 09/10/04 0:32 wfg <br />Chromium, total M200.7 ICP U mg/L 0.01 0.05 09/09/0415:36 wtg <br />Chromium, Trivalent Calculation (Total -Hexavalenl) U mg/L 0.01 0.05 09/21/04 15:08 wlc <br />Copper, total M200.7 ICP U mg/L 0.01 0.05 09/09/04 15:36 wlg <br />Iron, dissolved M200.71CP 0.02 B mg/L 0.01 0.05 09/10!04 0:32 wtg <br />Iron, total M200.7 ICP 0.43 ' mg/L 0.01 0.05 09109104 15:36 wlg <br />Lead, total M200.8 ICP-MS 0.0004 B mglL 0.0001 0.0005 09116104 14:08 scp <br />Magnesium, dissolved M200.7 ICP 3.5 mg/L 0.2 1 09110/04 0:32 wfg <br />Manganese, dissolved M200.7 ICP U mg/L 0.005 0.03 09/10(04 0:32 wfg <br />Manganese, total M200.7 ICP 0.023 B mglL 0.005 0.03 09109/04 15:36 wfg <br />Mercury, total M245.1 CVAA U mg/L 0.0002 0.001 09113/04 10:40 ak <br />Nickel, total M200.7 ICP U mg/L 0.01 0.05 09109104 15:36 wfg <br />Selenium, total SM 3114 B, AA•Hydride U mglL 0.001 0.005 09/17/04 11:53 Ijc <br />Silver, total M200.8 ICP-MS U mg/L 5E-OS 0.0003 09117104 19:21 scp <br />Zinc, total M200.7 ICP U mg/L 0.01 0.05 09/09/04 15:36 wrg <br />Metals Prep <br /> <br />Tofal Hot Plate M200.2 ICP 09/08104 10:46 ak <br />DigesBon <br />Totai Hof Plate M200.2 tCP-MS 09/08!04 6:50 scp/gjl <br />Digestion <br />Wel Chemistry <br /> <br />Chloride M325.2 - Colodmetric 2 B mg/L 1 5 09/08/04 18:37 jr <br />Chromium, Hexavalenl SM35000r-D U mglL 0.005 0.03 08/26104 13:11 mah <br />Cyanide, total M335.4 - Colodmetric wl distillation U mg/L 0.01 0.05 08131/04 15:52 ccp <br />Hardness as CaC03 SM2340B-Calculation 66 mg/L 1 7 09121/0415:08 calc <br />Lab Filtration SM 3030 B 08126104 13:07 mah <br />Lab Filtration & SM 3030 B 08/31/04 17:27 ak <br />Acidification <br />Nitrate as N, dissolved Calculation: N03N02 minus N02 0.08 B mg/L 0.02 0,1 09121/04 15:08 wlc <br />NitratelNitdte as N, M353.2 -Automated Cadmium 0.08 B mg/L 0.02 0,1 08127104 0:17 jr <br />dissolved Reduction <br />Nitrite as N, dissolved M353.2 -Automated Cadmium U mg/L 0.01 0.05 08/27104 0:17 jr <br /> ReducBon <br />Nitrogen, ammonia M350.1 -Automated Phenale U mg/L 0.05 0.5 09116/04 21:44 jr <br />pH (lab) M150.1 - Electrometdc 6.9 H units 0.1 0.1 08/30/04 12:44 mah <br />Residue, Filterable M160.1 - Gravimetric 140 mg/L 10 20 08/31/04 18:56 ct <br />(TDS) @1 BOC <br />Sulfate M375.3 - Gmvimefric 20 B mg/L 10 50 09/09!04 9:23 jah <br />Sulfide as S M376.2 -Methylene Blue U mg/L 0.02 0.1 09/01/04 14:12 mah <br />REPIN.01.11.00.01 • Please refer to Extended Qualifier Report for detail. <br />Bear Coal Company ACZ Sample ID: L47426.01 <br />Project ID: Date Sampled: 08/25/04 13:50 <br />Sample ID: N.F. GUNNISON-UPPER Date Received: 08/26/04 <br />Sample Matrix: Surface Water <br />