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ENERGY LABORATOR/ES, /NC. • 2393 Salt Creek Highway (82601) • P.O. Box 3258 • Casper, WY82602 .Toll FreeB8B.2350515 • 3072350515 • Fax 307234.1639 • casper@energylab.com • wwwenergylab.com QA/QC Summary Report Client: Cotter Corporation Report Date: 04/28/05 Project: JD-9 Work Order; 005040583 Analyte Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Methotl: SW6020 Batch: 7722 Sample ID: MB-7722 Method Blank 04/18/05 20:54 Antimony ND mg/L 0.00009 Arsenic ND mg/L 0.0002 Badum 0.001 mg/L 0.00008 Cadmium 0.0002 mg/L 0.0001 Chromium ND mg/L 0.00009 Copper 0.0009 mg/L 0.0001 lead 0.00005 mg/L 0.00004 Manganese 0.0002 mg/L 0.00008 Mercury ND mg/L 5.0E-06 Nickel 0.0004 mg/L 0.0002 Selenium ND mg/L 0.0006 Silver ~ 0.0002 mg/L 0,00008 Thallium ND mg/L 0.00007 Uranium 0.0001 mg/L 0,00008 Zinc 0.002 mg/L 1.0E-06 Sample ID: 005040583-001 AMS4 Post DigesOon Spike 04/18/05 21:09 Antimony 0.053 mg/L 7.2 99.6 75 125 Arsenic 0.26 mg/L 0.025 75 125 A Barium 0.31 mg/L 2.5 75 125 A Cadmium 0.050 mg/L 0.025 99.1 75 125 Chromium 0.051 mg/L 0.25 101 75 125 Copper 0.054 mg/L 0.25 91.6 75 125 Lead 0.075 mg/L 0.25 104 75 125 Manganese 0.099 mg/L 0.25 106 75 125 Mercury O.D047 mg/L 0.025 93.6 75 125 Nickel 0.062 mg/L 0.25 95.4 75 125 Selenium 0.11 mg/L 0.025 103 75 125 Silver 0.018 mg/L 0.12 35.1 75 125 S Thallium 0.049 mg/L 2.5 97.9 75 125 Uranium 0.32 mg/L 0.025 75 125 A Zinc 0.054 mg/L 0.25 99.9 75 125 -Matrix spike recoveries outside the acceptance criteria of 7510125 percent ar e considered matdx related, not system relatetl. Reported values are within mothod specifcations. Sample ID: 005040583-001AMSD4 Post Digestion Spike Dup 04/18/0521:18 Antimony 0.052 mg/L 1.2 98.6 75 125 0 20 Arsenic 0.26 mg/L 0.025 75 125 0.8 20 A Badum 0.33 mg/L 2.5 75 125 0 20 A Cadmium 0.049 mg/L 0.025 96.6 75 125 2.5 20 Chromium 0.050 mg/L 0.25 99.6 75 125 0 20 Copper 0.055 mg/L 0.25 93.3 75 125 0 20 QualiOers: RL-Analyle reporting limit. ND -Not detected at the reporOng limit. A -The analyte level was greater than four times the spike level. fn accordance with the method % recovery is not calculated. S -Spike recovery outside of advisory limits.