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1992-11-01_REVISION - M1988112
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1992-11-01_REVISION - M1988112
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Entry Properties
Last modified
6/20/2021 6:22:23 AM
Creation date
11/21/2007 9:02:06 PM
Metadata
Fields
Template:
DRMS Permit Index
Permit No
M1988112
IBM Index Class Name
Revision
Doc Date
11/1/1992
Doc Name
QUALITY ASSURANCE QUALITY CONTROL PROTOCOLS FOR THE COLLECTION OF SURFACE & GROUND WATER QUALITY DA
Type & Sequence
TR6
Media Type
D
Archive
No
Tags
DRMS Re-OCR
Description:
Signifies Re-OCR Process Performed
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<br />' procedures given in Section 5.3 for the ground water and surface <br />' water samples will apply. Quality control procedures for copper, <br />zinc, iron, calcium and sodium are the same as those given in <br />Section 5.3. <br />6.4.2 Total and WAD Cvanide Analvsis Onlv: The quality control protocols <br />for total cyanide analysis will be consistent with thosE described <br />in Section 5.3, subject to modification for the specific analytical <br />procedure, as described in USEPA Method 9010, Section 8, or USEPA <br />Method 9012, Section 8, given in Appendix G. WAD cyanide analyses <br />' in the process samples will follow similar protocols as the total <br />cyanide analyses. <br />' b.5 Analytical Accuracy and Verification <br />' 6.5.1 Full Analvsis: Analytical accuracy and verification protocols <br />' will be the same as described in Section 5.4 if there is sufficient <br />sample for analysis of all parameters listed in Table 2. <br />Analytical accuracy and verification procedures for copper, zinc, <br />iron, calcium and sodium analyses are the same as thos@ given in <br />Section 5.4. <br />Total and wAD cyanide analyses on the process sampled will be <br />' consistent with the protocols and data described in Section 6.5.2. <br />6.5.2 Total Cyanide Analy is Only; The analytical accuracy and <br />verification requirements will be similar to and consistent with <br />' Section 5.4. Limited data on accuracy and precision for total <br />cyanide analysis are given in USEPA Method 9010, Section 10. <br />The sensitivity of the manual method, USEPA Method 9010, using a <br />colorimetric finish, is given as 0.02 mg/L, suggesting a PQL of <br />' about 0.04 mg/L. The PQL for cyanide (all forms) in graund water <br />samples for the applicable, or most sensitive, analytical method is <br />' -42- <br /> <br />
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