ENFORCE37651

• Permit No: C1982056
• IBM Index Class Name: Enforcement
• Doc Date: 10/9/2006
• Doc Name: Analytical Results Report
• From: ACZ Laboratories
• To: DRMS
• Violation No.: CV2006006
• Media Type: D
• Archive: No

ACZ Laboratories, Inc.
Batch A distinct set of samples analyzetl at a specific time
Found Value of the OC Type of interest
Limit Upper limit for RPD, in %.
Lower Lower Recovery Limit, in % (except for LCSS, mgMg)
MDL McNOd Detection Limit. Same as Minimum Reporting Limit. Allows for instrument and annual Ouduations.
PCN/SCN A number assigned to reagents/standards to trace to the manufacturer's certifcate of analysis
POL Practical Ouandtation limit, typically 5 times the MDL.
OC True Value of the Control Sample or the amount atltled to the Spike
Rec Amount of the true value or spike added recovered. in % (except for LCSS, mg/Kg)
RPD Relative Pement Difference, calculation used for Duplicate OC Types
Upper Upper Recovery Limit, in % (except for LCSS, mg/Kg)
Sample Value of the Sample of interest
AS Analytical Spike (Post Digestion) LCSWD Laboratory ConVOI Sample -Water Duplicate
ASD Analybcal Spike (Post Digestion) Duplicate LFB Labomtory FortiFled Blank
CCB Continuing Calibration Blank LFM Laboratory Fortifed Matdx
CCV Continuing Calivation Verification standard LFMD laboratory Fortifed Matrix Duplicate
DUP Sample Duplicate LRB Laboratory Reagent Blank
ICB Initial Calibration Blank MS Matrix Spike
ICV Initial Calibration Verifcation standard MSD Matdx Spike Duplicate
ICSAB Inter-element Correction Standartl - A plus B solutions PBS Prep Blank -Soil
LCSS Laboratory Control Sample -Soil PBW Prep Blank -Water
LCSSD Laboratory Control Sample -Soil Duplicate POV Practical Ouantitation Verifcetion standard
LCSW Laboratory Control Sample -Water SOL Serial Dilution
Blanks Venfes that there is no or minimal contamination in the prep method or calibration procedure.
Control Samples Verifies the accuracy of the method, including th e prep procetlura.
Duplicates Verifies the precision of the insWmen[ and/or method.
Spikes/Fortifed Matrix Datertnines sample matrix intederences, if any.
Standard Verdes the validity of the calibration.
B Analyte concentration tletected at a value between MDL and POL,
H Analysis exceeded method hold time. pH is a field test with an immediate hold 6me.
R Poor spike recovery accepted because the other spike in the set fell within the given limits.
T High Relative Percent Difference (RPD) accepted because sample concentrations are less than 10x the MDL.
U Analyle was analyzed far but not tletected at the indiwtetl MDL
V High blank tlata accepted because sample concentration is 10 Bmes higher than blank concentmtion
W Poor recevery for Silver quality control is acceptetl because Silver often precipitates with Chloride.
X duality control sample is out of control.
Z Poor spike recovery is accepted because sample cencentretion is four times greater than spike concentration.
(1) EPA 600/4-83-020. Methods for Chemical Analysis of Water and Wastes, March 1983.
(2) EPA 600/R-93-100. Methods for the Determination of Inorganic Substances in Environmental Samples, August 1993.
(3) EPA 600/R-94-111. Methods for the Determination of Metals in Environmental Samples -Supplement I, May 1994.
(5) EPA SW-846. Test Methods for Evaluating Solid Waste, Thirtl Edition with Update III, December 1996.
(6) Standard Memods for the Examination of Water and Wastewater, 19N edition, 1995.
(1) QC results calculated from raw data. Results may vary slightly it the rounded values are used in the calculations.
(2) Soil, Sludge, and Plant matrices for Inorganic analyses are reported on a dry weight basis.
(3) Animal matrices for Inorganic analyses are reported on an "as received" basis.
REPIN03.11.00.01
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