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ii~~ CORE LABORATORIES D U A L I T Y C O N T R O L R E S U L T S Job Number.: 982396 Report Date.: 10/19/98 CUSTOMER: Greystone PROJECT: OTRY 484-03 AiTN: Jeff Spinzig Test Method........: EPA 200.7 Batch .............: 39063 Analyst...: Imt Method Description.: Netals Anal ysis(ICAP ), Trace Units .............: mg/L Parameter..........: Iron (Fe) OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result • Limits Dale Time MSD 982424-1 9808255 47.03836 41.12221 1.00 44.37496 266.3 X 80-120 09/14/1998 1553 13.4 R 20 PDS 982424-1 9808255 43.63956 1.00 44.37496 -73.5 X 75-125 09/14/1998 1556 PSD 982424-1 9808255 43.83415 43.63956 1.00 44.37496 -54.1 X 75-125 09/14/1998 1559 0.4 R 20 CCV 980912V 9.97690 10.0 99.8 X 90-110 09/14/1998 1602 CCB 9809148 0.01233 0,03 09/14/1998 1607 LCS 980676 50.84449 77.600000 65.5 X 37.2-162.4 09/14/1998 1614 SB 9808255 0.88192 1.00 88.2 X 75-125 09/14/1998 1618 CCV 980912V 9.94172 10.0 94.4 X 90-110 09/14/1998 1643 CCB 9809148 0.00739 0.03 09/14/1998 1647 ISR 980817E 89.62327 99.9075 89.7 X 80-120 09/14/1998 1701 ISB 980914M 84.88510 94.6125 89.7 X 80-120 09/14/1998 1704 CCV 980912V 9.77437 10.0 97.7 X 90-110 09/14/1998 1707 CCB 9809148 0.00866 0,03 09/14/1998 1718 Test Method........: EPA 239.2 Batch .............: 39066 Analyst...: kem Method Description.: Lead (GFAA) Units .............: mg/L Parameter..........: Lead (Pb) DC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result ' Limits Date Time ICV 980914V 0.04282 0.040000 107.0 X 90-110 09/14/1998 1744 ICB 09148 -0.00029 0,002 09/14/1998 1750 IDL a 20PP8 0.02192 09/14/1998 7756 IDL g 20PPB 0.02127 09/14/1998 1803 iDL is 20PPB 0.02792 09/14/1998 1809 IDL a 20PPB 0.02151 09/14/1998 1815 IDL g 20PPB -0.00078 09/14/1998 1821 IDL a 20PPB 0.02243 09/14/1998 1828 CCV 9809140 0.05457 0.050000 109.1 X 90-770 09/14/1998 7834 CC8 09148 -0.00090 0.002 09/14/1998 1840 MB 910 -0.00028 0.002 09/14/1998 1846 SB 980826) 0.02006 0.020000 100.3 X 75-125 09/14/1998 1853 MS 982378-1 980826) 0.02073 0.020000 0.00022 102.5 X 80-120 09/14/1998 7911 MSD 982378-1 980826) 0.02089 0.02073 0.020000 0.00022 103.3 X 80-720 09/14/1998 1978 0.8 R 20 PDS 982378-1 980511x 0.02208 0.020000 0.00022 109.3 X 75-125 09/74/1998 7924 PSD 982378-1 980511H 0.02282 0.02208 0.020000 0.00022 173.0 X 75-125 09/14/1998 1930 3.3 R 20 CCV 9809140 0.05244 0.050000 104.9 X 90-170 09/14/1998 1949 CCB 09148 0.00007 0,002 09/14/1998 7955 5B 980826) 0.02143 0.020000 107.2 X 75-125 09/14/1998 2014 M5 982372-1 980826) 0.02192 0.020000 0.00072 106.0 X 80-120 09/14/1998 2045 MSD 982372-1 980826) 0.02205 0.02192 0.020000 0.00072 106.7 X 80-120 09/14/1998 2051 0.6 R 20 CCV 9809740 0.05388 0.050000 107.8 X 90-110 09/14/1998 2104 CCB 09148 -0.00034 0.002 09/74/1998 2110 MB 0914 -0.00020 0.002 09/14/1998 2206 SB 960826) 0.02254 0,020000 112.7 X 75-125 09/14/1998 2213 CCV 9809140 0.05362 0.050000 107.2 X 90-110 09/14/1998 2219 CCB 09748 -0.00051 0.002 09/14/1998 2225 Page 9 ' Y.=X REC, R=RPD, A=ABS Diff., D=X Diff.