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LWAG~'fB~, CORE LABORATORIES D U A L I T Y C O N T R O L R E S U L T S Job Number.: 982396 Report Date.: 10/19/98 CUSTOMER: Greystone PROJECT: DTRY 484-03 ATTN: Jeff Spinzig Test Method........: EPA 200.7 Batch .............: 39063 Analyst...: lmt Method Description.: Metals AnalyS is(1LAP ), Trace Units .............: mg/L Parameter..........: Barium (Ba) OL lab ID Reagent DC Result OC Result True Value Orig. Value Cal c. Result • Limi [s Date Time LLS 980676 0.84064 0.834000 100.8 X 77.1.123.5 09/14/1998 1614 SB 9808255 1.84275 2.00 92.1 X 75.125 09/14/1998 1618 CCV 980912V 5.06630 5.00 101.3 X 90-110 09/14/1998 1643 CCB 980974B 0.00029 0.001 09/14/1998 1647 PDS 982442-3 9808255 3.24281 2.00 1.26358 99.0 Y. 75.125 09/14/1998 1650 PSD 982442-3 9808255 3.24288 3.24281 2.00 1.26358 99.0 X 75-125 09/14/1998 1653 0.0 R 20 158 980914M 0.51191 0.4991 102.6 X 80.120 09/14/1998 1704 CCV 980912V 4.99940 5.00 100.0 X 90.110 09/14/1998 1707 LLB 9809148 0.00018 0.001 09/14/1998 1718 Test Methotl.. ......: EPA 200.7 Batch .............: 39063 Analyst...: lmt Method Description.: Metals Anal ysis(ICAP), Trace Units .............: mg/L Parameter..........: Iron (Fe) OL lab ID Reagent DC Result OC Result True Value Orig. Value Calc. Result ' Limits Date lime LRA 9808252 0.02258 09/14/1998 1045 LRA 9809142 0.02568 09/14/1998 1049 LRA 980814E 9.84641 10.000 09/14/1998 1052 LRA 980825R -0.03354 09/14/1998 1056 ICV 980912V 10.02950 10.0 100.3 X 90.110 09/14/1998 1107 !CB 9809148 0.00619 0.03 09/14/1998 1116 I5A 980817E 90.79563 99.9075 90.9 X 80.120 09/14/1998 1120 ISB 980914N 84.07502 94.6125 88.9 X 80-120 09/14/1998 1145 MB 0911 0.01855 0.03 09/14/1998 1153 lCS 980676 66.82519 77.600000 86.1 X 37.2.162.4 09/14/1998 1157 CCV 980912V 10.16825 10.0 101.7 X 90.110 09/14/1998 1220 CCB 9809148 0.00801 0.03 09/14/1998 1224 SB 9808255 1.02536 1.00 102.5 X 75.125 09/14/1998 1229 ISA 980817E 96.62916 99.9075 96.7 X 80.120 09/14/1998 1255 Ise 980914M 88.86197 94.6125 93.9 X 80.120 09/14/1998 1258 CCY 980912V 10.44934 10.0 104.5 X 90.110 09/14/1998 1301 CCB 9809146 0.01234 0.03 09/14/1998 1305 SB 9808255 1.05453 1.00 105.5 X 75-125 09/14/1998 1315 CCV 980912V 9.46916 10.0 94.7 X 90-110 09/14/1998 1358 CCB 9809148 0.00615 0.03 09/14/1998 1401 MB 0911 0.02227 0.03 09/14/1998 1418 SB 9808255 0.97673 1.00 97.7 X 75.125 09/14/1998 1421 MS 982414-1 9808255 1.06147 1.00 0.07154 99.0 X 80.120 09/14/1998 1428 M50 982414-1 9808255 1.05849 1.06147 1.00 0.07154 98.7 X 80-120 09/14/1998 1431 0.3 R 20 CCV 980912V 10.43976 10.0 104.4 X 90.110 09/14/1998 1438 CCB 9809148 0.0098d 0.03 09/14/1998 1442 SD 982394-4 0.01545 0.02656 09/14/1998 1455 MB O9D3 0.01858 0.03 09/14/1998 1459 SB 9808255 1.10867 1.00 110.9 X 75.125 09/14/1998 1502 SB 9808255 0.96617 1.00 96.6 X 75.125 09/14/1998 1521 CCV 980912V 9.63642 10.0 96.4 X 90-110 09/14/1998 1524 CCB 980914B 0.01481 0.03 09/14/1998 1529 M8 0914 0.01732 0.03 09/14/1998 1532 MS 982424-1 9808255 41.12221 1.00 44.37496 -325.3 Y. 80.120 09/14/1998 1550 Page 8 ' X=Y. REC, R=RPD, A=ABS Diff., D=X Diff.