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fC~9E~' <br />CORE LABORATORIES <br />Q U A L I T Y C O N T R O L R E S U L T S <br />Job Number: 963307 Oate: 12/27/96 <br />WSTONER: Creystone PROJECT: 483.03 ~ .ATTN: ,Leff ~Spi nxig <br />Test Method........: EPA 204.2 ~. Batch ....:........: ~T6563 Analyst...: lmt <br />Method Description.: Antimony (GFAA) ~ ~ Reporting limit...: 6.003 <br />Parameter..........: Antimony (Sb) ~ ~ Units .............: alq/L <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time <br />!ID 963242-1 -0.00181 -0.00153 0.00028 ABS Diff. 12/16/96 1228 <br />MD 963307-1 -0.00032 -0.00174 0.00147 ABS Diff. 12/16/96 1247 <br />P05 963307-2 960716[ 0.01775 0.020000 -0.00121 94.8 X REC 12/16/96 1300 <br />C[V 960911[ 0.04930 0.050 98.6 X REC 12/16/96 1307 <br />CCB 12166 -0.00006 12/16/96 1313 <br />SD 963307-2 -0.00106 -0.00121 X Diff. 12/16/96 1319 <br />MB 1211 -0.00078 12/16/96 1326 <br />LCS 9612022 0.03655 0.040000 91.4 Y. 0.E[ 12116/96 1332 <br />MD 963318-1 -0.00062 -0.00048 0.00014 ABS Diff. 12/16/96 1345 <br />MS 963336-1 961002E 0.01846 0.020000 0.00028 90.9 X REC 12/16/96 1358 <br />EB 1312 -0.00073 12!16196 1405 <br />SB 9610024 0.02015 0.020000 100.8 % REC 12/16/96 1411 <br />CCV 960911[ 0.04846 0.050 96.9 X REC 12/16/96 1424 <br />CCB 12166 -0.00024 12/16/96 1430 <br />ED 963276-1 -0.00107 0.00052 0.00159 ABS Diff. 12/16/96 1437 <br />MS 963276-2 9610021 0.02028 0.020000 -0.00173 110.0 X REC 12/16/96 1450 <br />CCV 960911[ 0.04848 0.050 97.0 X REC 12/16196 1509 <br />CCB 12166 -0.00052 12/16/96 1516 <br />Test Method........: EPA 270.2 Batch .............: 16673 Analyst...: lmt <br />Method Description.: Selenium (GFAA) Reporting Limit...: 0.005 <br />Parameter..........: Selenium (Se) Units .............: mg/L <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time <br />ICV 9610098 0.03967 0.0400 X REC 12/18/96 0940 <br />ICB 12186 0.00004 12/18/96 0947 <br />CCV 961024[ 0.04539 0.050 90.8 X REC 12/18/96 1105 <br />CCB 12186 -0.00038 12/18/96 1112 <br />CCV 961029[ 0.04665 0.050 93.3 X REC 12!18196 1230 <br />[CB 12186 -0.00007 12/18/96 1237 <br />CCV 961029[ 0.05007 0.050 100.1 X REC 12/18/96 1401 <br />CCB 12188 -0.00027 12/18196 1409 <br />CCV 961029[ 0.05096 0.050 101.9 X REC 12/18/96 1444 <br />CCB 12186 -0.00058 12/18/96 1451 <br />CCV 961029[ 0.04654 0.050 93.1 X REC 12118196 1609 <br />CCB 12186 -0.00025 12/18/96 1616 <br />[CV 961029[ 0.05136 0.050 102.7 X REC 12/18/96 1733 <br />CCB 12186 -0.00046 12!18!96 1740 <br />CCV 961029[ 0.05193 0.050 103.9 X REC 12/18/96 1858 <br />CCB 12186 -0.00019 12/18/96 1905 <br />[CV 961029[ 0.04737 0.050 94.7 X REC 12/18/96 1948 <br />CCB 12186 -0.00115 12/18/96 1955 <br />MID 963307-1 -0.00098 0.00024 0.00122 ABS Di ff. 12/18/96 2030 <br />SD 963307-1 -0.00030 0.00024 X Di ff. 12/18/96 2037 <br />PDS 963307-2 960912H 0.01969 0.020000 -0.00022 99.5 X REC 12/18/96 2051 <br />CCV 9610290 0.04770 0.050 95.4 X REC 12/18/96 2134 <br />CCB 12186 -0.00012 12/18/96 2141 <br />Page 25 <br />