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I~E~; <br />CORE LABORATORIES <br />Q U A L I T Y C O N T R O L R E S U L T S <br />Job Number: 963307 Date: 12!27/96 <br />CUSTOMER: ~Creystone ~ PROJECT: 483.03 ATTN: Jeff Spinxig <br />Tesc.Methad........: EPA 279.2 ~ Batch .............: 16450 Analyst...: lmt <br />Method Description.: Thalliun (GFAA) Reportin4 Limit.,.: 0,005 <br />Parameter..........: Thalt ium iTl) Units .............: mg/L <br />OC Lab ID Reagent OC Result <br />CCB 12126 0.00089 <br />ED 963276-1 0.00031 <br />MD 963276-1 0.00030 <br />MS 963276-2 961002E 0.02232 <br />LC5 9612022 0.03723 <br />MD 963318-1 0.00069 <br />MS 963336-1 961002E 0.01777 <br />CCV 961029[ 0.04999 <br />CCB 12126 -0.00011 <br />CCV 9610290 0.05204 <br />CC8 12126 0.00130 <br />MD 963307-1 0.00002 <br />SD 963307-1 0.00092 <br />POS 963307-2 960912H 0.02060 <br />CCV 961029[ 0.05200 <br />ct8 12126 0.00033 <br />OC Result True Value Orig. Value Ca lc. Result Units Date/Time <br /> 12/12/96 1238 <br /> 0.00023 0,00008 A85 Diff. 12/12/96 1253 <br /> 0.00023 0.00007 ABS Diff. 12/72/96 1301 <br />0.020000 0.00081 107.5 X REC 12/12/96 1316 <br />0.040000 93.1 X REC 12112!96 1323 <br /> 0.00059 0.00070 ABS Diff. 12/12/96 1338 <br />0,020000 0.00009 88.4 X REC 12/12/96 1353 <br />0.050 100.0 X REC 12!12!96 1400 <br /> 12/12/96 1408 <br />0.050 104.1 X REC 12/12/96 1415 <br /> 72/12!96 7423 <br /> -0.00008 0.00010 ABS Diff. 72/12/96 1438 <br /> -0.00008 X Diff. 12/12!96 1445 <br />0.020000 0.00037 101.2 X REC 72/72!96 1500 <br />0.050 104.0 X REC 12/12/96 1508 <br />12/12)96 7575 <br />Test Method........: EPA 420.1 Batch .............: 16525 Analyst...: dem <br />Method Oescri pt ion.: Phenols, Total Recoverable Reporting Limit..,: 0.05 <br />Parameter....,.....: Ph eno t, Total Recoverable Units .............: mg/L <br />DC Lab ID Reagent DC Result OC Result True Value Orig. Value Calc. Result Units Date/Time <br />ttl 960067 0.03 0.05 60.0 X REC 12116!96 0900 <br />ICB 0.00 12/76/96 0900 <br />MB 0.00 12/76/96 0900 <br />MD 963300-1 0.00 0,01 0.01 ABS Diff. 12116/96 0900 <br />XS 963300-1 G961015C 0.27 0.250000 0,01 80.0 % REC 72/16/96 0900 <br />CCV G961015C 0.48 0.500000 96.0 X REC 12/76/96 0900 <br />CCB 0.00 12/76/46 0900 <br />CCV G961015C 0,49 0.500000 98.0 X REC 12/16/96 0900 <br />CCB 0.00 12/16/96 0900 <br />Test Method........: EPA 204.2 Batch .............: 16563 Analyst...: Imt <br />Nethod Description.: Antimony (GPAA) Reporting Limit...: 0.003 <br />Parameter..........: Antimony (56) Units .............: mg/L <br />OC Lab [D Reagent OC Result OC Result True Value Orig. Value Calc. Result <br />1CV 9609118 0.04200 0.0400 105,0 <br />ICB 12166 0.00111 <br />CCV 960911[ 0.04911 0,050 98.2 <br />CCB 12166 -0.00021 <br />CCV 960911[ 0.04441 0.050 98.9 <br />CCB 12166 -0.00081 <br />SD 963188-9 -0.00119 -0,00018 <br />CCV 960911[ 0.04989 0.050 99.8 <br />CCB 12166 -0.00236 <br />MB 1205 -0.00107 <br />LC5 961017H 0.03469 0.040000 86.7 <br />M5 963242-7 961002E 0.02006 0.020000 -0.00153 108.0 <br />Uni [s Date/Time <br />X REC 12/16196 0842 <br />12/16/96 0848 <br />X REC 12/16/96 0959 <br />12/16!96 1006 <br />X REC 12/16/96 1117 <br />12/16/96 1123 <br />X Diff- 12/16/96 1143 <br />X REC 12/16/96 1149 <br />12/16/96 1156 <br />12!16/96 1202 <br />X REC 12/16/96 1208 <br />X REC 12116/96 1221 <br />Page 24 <br />