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C~E~ <br />CORE LABORATORIES <br />D U A L I T Y C O N T R O L R E S U L T S <br />Job Number: 963307 Date: 12/27/96 <br />CUSTOMER: Greystone: ~:. ~ ~~~~PROJECT.;: 483-OS ~ ~.~ ATTN~;. Jeff Spinxig <br />Test Method........; EPA 200.7 ~~.~:~~ ~ Batch;... _....:...:.: 16403 ~ Analyst...: smh <br />Method Description.: Metals AnalysisCtCAP ), Trace ~ ~Reporting limit :..:: 0.01 <br />~ <br />Parameter ..........:. .8erium .CBa) .~ .~ :. . .~~~ .~~:~Ilnits~....:..~...:..:~mg/L~ . <br />. <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time <br />ICV 9b0678Y 2.09644 2.00 104.8 % REC 12111)96 1056 <br />ICB 9611142 0.00043 12/11/96 1116 <br />ISB 960929R 0.45197 0.5000 90.4 X REC 12/11/96 1135 <br />CCV 9610222 5.05136 5.0 101.0 X REC 12/17/96 1324 <br />CCB 9611142 0.00099 12111!96 1339 <br />MD 963282-1 0.00741 0.00755 0.00014 ABS Diff. 12111/96 1357 <br />PDS 963282-1 9611060 0.48229 1.000 0.00755 97.5 X REC 12/11/96 1406 <br />MD 963296-1 0.03768 0.03778 0.00010 A85 Diff. 12/11/96 1430 <br />CCV 9610222 5.04742 5.0 100.9 X REC 12/11/96 1441 <br />CCB 9611142 0.00078 12!11196 1452 <br />PDS 963296-3 9611060 1.14776 1.000 0.18755 96.0 X REC 12/11/96 1500 <br />CCV 9610222 5.09763 5.0 102.0 X REC 12/11/96 1552 <br />CCB 9611142 0.00017 12/11/96 1607 <br />[SB 960429R 0.44495 0.5000 89.0 X REC 12111)46 1618 <br />CCV 9610222 5.15524 5.0 103.1 X REC 72/11/96 1632 <br />CCB 9611142 0.00052 12/11/96 1646 <br />CCV 9610222 5.19482 5.0 103.9 X REC 12/11)96 1858 <br />CCB 9611142 -0.00000 12/11146 2007 <br />CCV 9610222 5.02967 5.0 100.6 X REC 12/11/96 2128 <br />CCB 9611142 0.00002 12/11/96 2156 <br />CCV 9610222 4.94281 5.0 98.4 Y. REC 12/11/96 2307 <br />CCB 9611142 0.00027 12!11/46 2320 <br />CCV 9610222 4.90544 5.0 98.1 Y. REC 12/12/96 0029 <br />CCB 9611142 0.00041 12/12/96 0042 <br />CC4 9610222 5.05924 5.0 101.2 X REC 12/12/96 0129 <br />CCB 9611142 -0.00002 12!12!96 0146 <br />ISB 960929R 0.50650 0.5000 101.3 X REC 12/12/96 0215 <br />CCV 9610222 5.14184 5.0 102.8 X REC 72/12/96 0225 <br />CCB 9611142 -0.00084 12/12/96 0237 <br />Test Method........: EPA 200.7 Ba CCh.~ .. . :........: 16403 ~ Analyst...: smh <br />Method Description.; Metals Anal ysis(ICAP), Trace Reporting .L imit.:.: 0.002 <br />Parameter..........: Beryllium (Bel ~ ~ units .............: mg/L <br />OC Lab ID Reagent OC Result <br />ICV 961106Y 2.08774 <br />!CB 9611142 0.00046 <br />ISB 960929R 0.49501 <br />CCV 9610222 2.49234 <br />CC8 9611142 0.00034 <br />~ 963282-1 0.00009 <br />PDS 963282-1 9611060 0.99273 <br />MD 963296-t 0.00005 <br />CCV 9610222 2.52787 <br />CC8 9611142 0.00012 <br />PDS 963296-3 9611060 0.99959 <br />CCV 9610222 2.59121 <br />CCB 9611142 0.00041 <br />ISB 960929R 0.51276 <br />CCV 9610222 2.60876 <br />CCB 9611142 0.00046 <br />DC Result True Value Drig. Value Calc. Result Units Date/Time <br />2.00 104.4 X REC 12!71!96 1018 <br /> 12/11/96 1116 <br />0.5000 99.0 X REC 12/11/96 1135 <br />2.5 99.7 X REC 12/71/96 1324 <br /> 12/11/96 7339 <br /> 0.00009 0.00000 ABS Diff. 72/11/96 1357 <br />7.000 0.00009 99.3 X REC 12/11/96 1406 <br /> 0.00003 0.00002 ABS Diff. 12711196 1430 <br />2.5 701.7 X REC 12/11/96 1441 <br /> 12/11/96 7452 <br />7.000 -0.00021 100.0 X REC 12/71/96 1500 <br />2.5 103.6 X REC 12/11/96 1552 <br /> 72/71/96 7607 <br />0.5000 702.6 X REC 12/11/96 1618 <br />2.5 104.4 X REC 12/11/96 1632 <br /> 12!11!96 1646 <br />Page 17 <br />