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~~ <br />CORE LABORATORIES <br />D U A L I T Y C O N T R O L R E S U L T S <br />Jab Number: 963307 Oate: 12/27!96 <br />CUSLOMER: Grrystone ~ ~ ~ PROJECT: 483-03 ~ .ATTN: Jeff.~Spintig <br />Test Method........: EPA 335.2 ~ ~ ~ ~ Batch .:...........: .t6345 ~ AnalYst...: dme <br />Method.Descri ption.:~ Cyani de, Total (Tit., Spec.) ~. ~ ~~Reporting Limit ..:: 0.02' <br />Parameter..........: CYani de, Total ~ ~ ~ ~ Units ..:....... .::: mg/L <br />OC Lab ID Reagent OC Resul[ OC Result True Value Orig. Value Cal c. Result Units Date/Time <br />ICV G9611058 0.457 0.500000 91.4 X REC 12/10/96 1240 <br />ICB 0.000 72/10/96 1240 <br />DSC G961105A 0.793 0.200000 96.5 X REC 12/10/96 1240 <br />MB 0.000 12/10/96 1240 <br />MD 963286.1 0.000 0.000 D ABS Diff. 12110/96 1240 <br />MS 963286-1 G961105A 0.245 0.250000 0.000 98.0 X REC 12/10/96 1240 <br />CCV C961105A 0.307 0.300003 102.3 X REC 12/10/96 1240 <br />CCB 0.000 12/10/96 1240 <br />Test Method........: EPA 200.7 Batch ..... ........: 16403 Analyst...: smh <br />Method Description.: Metals Analysi s(ILAP), Trace Reporting Limit...: 0.05 <br />Parameter..........: Arsenic (AS) Units .............: mg/L <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time <br />ICV 961106Y 2.08038 2.00 104.0 X REC 12/17/96 1018 <br />ICB 9611142 -0.00004 12(11!46 7116 <br />ISB 9609298 1.01278 1.000 701.3 X REC 12/11/96 1135 <br />CCV 9610222 2.55479 2.5 102.2 y. REC 12!11/96 1324 <br />CCB 9611142 -0.00216 72/11/96 1339 <br />MD 963282-1 0.00097 0.00155 0.00058 ABS Diff. 12/11/96 1357 <br />PDS 963282.1 9677060 0.98505 1.000 0.00155 98.3 X REC 12/11/96 1406 <br />MD 963296.1 0.00530 0.00277 0.00313 ABS Diff. 12/11/96 1430 <br />CCV 9610222 2.57185 2.8 102.9 X REC 12/11/96 1441 <br />CCB 9617142 -0.00108 12/11/96 1452 <br />PDS 963296.3 9611060 1.01610 7.000 0.00088 101.5 X REC 72/71/96 1500 <br />CCV 9610222 2.57707 2.5 103.1 X REC 12/11/96 1552 <br />CCB 9611142 -0.00089 72/11/96 1607 <br />ISB 9609298 1.00679 1.000 100.7 X REC 12/11/96 1618 <br />CCV 9610222 2.60090 2.8 104.0 X REC 12/11/96 1632 <br />CCB 9611142 0.00108 12/11/96 1646 <br />CCV 9610222 2.60156 2.5 104.1 X REC 12/11/96 1858 <br />CCB 9611142 0.00274 12/11/96 2007 <br />CCV 9610222 2.62157 2.5 104.9 X REC 12!11!96 2128 <br />CCB 9611142 -0.00200 12/11/96 2156 <br />CCV 9610222 2.61747 2.8 104.7 X REC 12711!96 2307 <br />CCB 9611142 0.00054 72/11/96 2320 <br />CCV 9610222 2.61689 2.5 104.7 X REC 72/12796 0029 <br />CC8 9611142 0.00192 12/72/96 0042 <br />CCV 9610222 2.55137 2.5 102.1 X REC 12!12196 0129 <br />CCB 9611142 •0.00089 12/72/96 0746 <br />ISB 9609298 0.95644 7.000 95.6 X REC 12/72/96 0275 <br />CCV 9610222 2.51198 2.5 100.5 X REC 12/12/96 0225 <br />CC8 9611142 •0.00090 12/12/96 0237 <br />Page 1b <br />