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MATRL4 SPIRE SAMPLE DATA REPORT <br />General Chemistry <br />Client Lot #...: D4D090366 Matrix.........: WATER <br />Date Sampled...: 04/08/04 08:24 Date Received..: 04/09/04 <br />SAMPLE SPIKE MEASRD PERCNT PREPARATION- PREP <br />PARAMETER AMOIINT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE BATCH # <br />Ammonia as N WO#: GDWAAlEF -MS/GDWAAlEG-MSD MS Lot-Sample #: D4D090228 -001 <br />ND 4.00 3.88 mg/L 96 MCAWW 350.1 04/14/04 4105426 <br />ND 4.00 3.83 mg/L 95 1.2 MCAWW 350.1 04/14/04 4105426 <br /> Dilution Factor: 1 <br /> Analysis Time..: 01:00 <br />Nitrate-Nitrite WO#: GDW3C1C6 -MS/GDW3C1C7-MSD MS Lot-Sample #: D4D090301 -001 <br />0.030 4.00 2.97 mg/L 74 MCAWW 353.2 04/14/04 4105497 <br />0.030 4.00 2.98 mg/L 74 0.20 MCAWW 353.2 04/14/04 4105497 <br /> Dilution Factor: 1 <br /> Analysis Time..: 01:00 <br />Nitrite WO#: GDXRDIDH -MS/GDXRDIDJ-MSD MS Lot-Sample #: D4D090366 -001 <br />0.58 0.500 0.935 mg/L 71 MCAWW 353.2 04/10/04 4102099 <br />0.58 0.500 0.925 N mg/L 69 1.1 MCAWW 353.2 04/10/04 4102099 <br /> Dilution Factor: 1 <br /> Analysis Time..: 17:45 <br />Sulfate WO#: GDWAAICP -MS/GDWAAICQ-MSD MS Lot-Sample #: D4D090228- 001 <br />220 250 489 I mg/L 110 MCAWW 375.4 04/16/04 4107635 <br />220 250 479 I mg/L 105 2.3 MCAWW 375.4 04/16/04 4107635 <br /> Dilution Factor: 1 <br /> Analysis Time..: 11:00 <br />Calculations are performed before rouMing to avoid rountl-off ertors in calculated results. <br />N Spiked analyze recovery is outside salted ventral limits. <br />I Estimated result. Result concentration exceeds the calibration range. <br />38 <br />