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MATRIR SPIRE SAMPLE HVALDATION REPORT <br />General Chemistry <br />Client Lot #...: D4D090366 <br />Date Sampled...: 04/08/04 08:24 Date Received..: 04/09/04 <br />PERCENT RECOVERY RPD <br />PARAMETER RECOVERY LIMITS RPD LIMITS METHOD <br />Ammonia as N WO#: GDWAAlEF-MS/GDWAAlEG-MSD <br />96 (44 - 130) MCAWW 350.1 <br />95 (44 - 130) 1.2 (0-30) MCAWW 350.1 <br />Dilution Factor: 1 <br />Analysis Time..: 01:00 <br />Matrix.........: WATER <br />PREPARATION- PREP <br />_ ANALYSIS DATE BATCH # <br />MS Lot-Sample #: D4D090228-001 <br />04/14/04 4105426 <br />04/14/04 4105426 <br />Nitrate-Nitrite WO#: GDW3C1C6-MS/GDW3C1C7-MSD MS Lot-Sample #: D4D090301-001 <br />74 (62 - 119) MCAWW 353.2 04/14/04 4105497 <br />74 (62 - 119) 0.20 (0-30) MCAWW 353.2 04/14/04 4105497 <br /> Dilution Factor: 1 <br /> Analysis Time..: 01:00 <br />Nitrite WO#: GDXRDIDH-MS/GDXRDIDS-MSD MS Lot-Sample #: D4D090366-001 <br />71 (71 - 122) MCAWW 353.2 04/10/04 4102099 <br />69 N (71 - 122) 1.1 (0-20) MCAWW 353.2 04/10/04 4102099 <br /> Dilution Factor: 1 <br /> Analyais Time..: 17:45 <br />Sulfate WO#: GDWAAICP-MS/GDWAAICQ-MSD MS Lot-Sample #: D4D090228-001 <br />110 I (56 - 129) MCAWW 375.4 04/16/04 4107635 <br />lOS I (56 - 129) 2.3 (0-15) MCAWW 375.4 04/16/04 4107635 <br /> Dilution Factor: 1 <br /> Analyais Time..: 11:00 <br />Calculations are performed before rounding to avoid round-off errors in calculated resulu. <br />N Spiked analyze recovery is outside sUted control limits. <br />I Estimated result. Result concentration exceeds Ne calibm[ion range. <br />37 <br />