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MATRIR SPIRE SAMPLE DATA REPORT <br />TOTAL Metals <br />Client Lot #...: D4D090366 Matrix.........: WATER <br />Date Sampled...: 04/09/04 15:40 Date Received..: 04/09/04 <br />SAMPLE SPIKE MEASRD PERCNT PREPARATION- WORK <br />PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE ORDER # <br />Thallium <br />0.00016 0.0400 0.0455 mg/L 113 MCAWW 200.8 04/15-04/19/04 GDXRDICQ <br />0.00016 0.0400 0.0458 mg/L 114 0.57 MCAWW 200.8 04/15-04/19/04 GDXRDICR <br />Dilution Pactor: 1 <br />Analysis Time..: 19:02 <br />Vanadium <br />ND 0.0400 0.0536 mg/L 132 <br />Qualifiers: N <br />ND 0.0400 0.0534 mg/L 131 <br />Qualifiers: N <br />Dilution Factor: 1 <br />Analysis Time..: 19:02 <br />Zinc <br />MCAWW 200.8 04/15-04/19/04 GDXRDICX <br />0.42 MCAWW 200.8 04/15-04/19/04 GDXRDICO <br />0.011 0.0400 0.0534 mg/L 107 MCAWW 200.8 04/15-04/19/04 GDXRDICE <br />0.011 0.0400 0.0529 mg/L 105 0.88 MCAW'A 200.8 04/15-04/19/04 GDXRDICF <br />Dilution Factor: 1 <br />Analysis Time..: 19:02 <br />Calculations are pertormed before rounding ro avoid round-off errors in calculated reruns. <br />N Spiked analyze recovery is outside stated con[ml limits. <br />NC The recovery and/or RPD were not ralculated. <br />MSH The rewvery and RPD were not ralculated because the sample amount was greater thzn four times the spike amount. <br />2a <br />