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MATRI% SPIKE SAMPLE DATA REPORT <br />TOTAL Metals <br />Client Lot #...: 040090366 Matrix.........: WATfiR <br />Date Sampled...: 04/09/04 15:40 Date Received..: 04/09/04 <br />SAMPLE SPIKE MEASRD PERCNT PREPARATION- WORK <br />PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE ORDER # <br />MS Lot-Sample #: 040090366-001 Prep Batch #...; 4105630 <br />Antimony <br />0.00033 0.0400 0.0462 mg/L 115 MCAWW 200.8 04/15-04/19/04 GDXRDICI. <br />0.00033 0.0400 0.0452 mg/L 112 2.2 MCAWW 200.8 04/15-04/19/04 GDXRDICK. <br />Dilution Factor: 1 <br />Analysis Time..: 19:02 <br />Arsenic <br />Barium <br />Lead <br />Selenium <br />0.013 0.0400 0.0646 mg/L 129 MCAWW 200.8 04/15-04/19/04 GDXRDIC7 <br />Qualifiers: N <br />0.013 0.0400 0.0664 mg/L 134 2.8 MCAWW 200.8 04/15-04/19/04 GDXRD1Cr <br />Qualifiers: N <br />Dilution Factor: 1 <br />Analysis Time..: 19:02 <br />0.026 0.0400 0.0734 mg/L 119 MCAWW 200,8 04/15-04/19/04 GDXRDICV <br />Qualifiers: N <br />0.026 0.0400 0.0725 mg/L 116 1.2 MCAWW 200,8 04/15-04/19/04 GDXRDI C4: <br />Dilution Factor: 1 <br />Analysis Time..: 19:02 <br />0.00031 0.0400 0.0449 mg/L 111 <br />0.00031 0.0400 0.0446 mg/L 111 <br />Dilution Factor: 1 <br />Analysis Time..: 19:02 <br />0.76 0.0400 0.851 mg/L <br />Qualifiers: NC,MSA <br />0.76 0.0400 0.832 mg/L <br />Qualifiers: NC, MSB <br />Dilution Factor: 1 <br />Analysis Time..: 19:02 <br />Silver <br />0.00003 0.0400 0.0415 mg/L 104 <br />0.00003 0.0400 0.0412 mg/L 103 <br />Dilution Factor: 1 <br />Analysis Time..: 19:02 <br />MCAWW 200.8 04/15-04/19/04 GDXRDICJ <br />0.61 MCAWW 200.8 04/15-04/19/04 GDXRDICK <br />MCAhW 200.8 04/15-04/19/04 GDXRD1Ch <br />MCAWW 200,8 04/15-04/19/04 GDXRDICY <br />MCAWW 200,8 04/15-04/19/04 GDXRDICG <br />0.68 MCAWW 200.8 04/15-04/19/04 GDXRDICY. <br />(Continued on next page) <br />2~ <br />