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WR@~' CORE LABORATORIES Q U A L I T Y C O N T R O L R E S U L T S Job Number: 962453 Date: 09/28/96 CUSTOMER: Greyst one PROJECT: 484-03 ATTN: Ray Faciski Test Method........: EPA 200.7 Batch .............: 13526 Analyst...: gag Method Description.: Meals Analysis(ILAP), Trace Reporting Limit...: 0.1 Parameter..........: Calcium (Ca) Units .............: mg/L OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time CCB 9608022 0.00246 09120196 1412 MD 962556-1 64.76550 63.83811 1.4 RPD 09/20/96 1451 PDS 962556-1 960917G 105.46778 50.000 63.83811 83.3 X REC 09/20/96 1456 CCV 9606272 102.01881 100.00 102.0 X REC 09/20/96 1519 CCB 9608022 0.00026 09/20/96 1533 CCV 9606272 101.03735 100.00 101.0 X REC 09/20/96 1626 CCB 9608022 -0.00233 09/20/96 1646 ISA 960323A 442.48382 500 88.5 X REC 09/20/96 1651 ISB 960630H 423.19287 500 84.6 X REC 09/20/96 1658 CCV 9606272 101.97227 100.00 102.0 X REC 09!20/46 1701 CCB 9608022 0.00023 09/20/96 1715 Tes[ Method........: EPA 200.7 Batch ............. : 13526 Analyst...: gag Method Oescript ion.: Meia(s Analysis(ICAP), Trace Reporting Limit... : 0.005 Parameter..........; Chromium (Cr) Units ............. : mg/L oC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time ICV 9606182 1.93225 2.00 96.6 X REC 09/20/96 0950 ICB 9608022 0.00026 09/20/96 1024 ISB 960630H 0.57477 0.5000 115.0 X REC 09/20/96 1046 MD 962449-1 0.00024 0.00131 0.00107 ABS Diff. 09/20/96 1312 PDS 962449-1 960917G 1.02043 1.000 0.00131 101.9 % REC 09/20/96 1322 CCV 9606107 2.45161 2.5 98.1 X REC 09/20/96 1343 CCB 9608022 -0.00069 09/20/96 1412 MD 962556-1 0.00000 0.00093 0.00093 ABS Diff. 09/20/96 1451 PDS 962556-1 960917G 0.95228 1.000 0.00093 95.1 X REC 09/20/96 1456 CCV 9608107 2.46136 2.5 98.5 X REC 09/20/96 1524 CCB 9608022 -0.00116 09/20/96 1533 CCV 9606107 2.42301 2.5 96.9 Y. REC 09/20/96 1636 CCB 9608022 -0.00185 09/20/96 1646 ISB 960630H 0.53732 0.5000 107.5 X REC 09R0l96 1658 CCV 9606107 2.45206 2.5 98.1 % REC 09/20/96 1705 CCB 9608022 -0.00069 09/20/96 1715 Test Method........: EPA 200.7 Batch .............: 13526 Analyst...: gag Method Description.: Metals Anal ysi s(ILAP), Trace Reporting Limit...: 0.03 Parameter..........: Iron (Fe) Units .............: mg/L OC Lab ID Reagent OC Resul[ OC Result True Value Orig. Value Calc. Resin[ Units Oate/Time ICV 9606182 2.09125 2.00 104.6 % REC 09/20/96 0950 ICB 9608022 0.01936 09/20/96 1024 ISA 960323A 210.18594 200 105.1 X REC 09/20/96 1031 ISB 960630H 205.23025 200 102.6 X REC 09/20/96 1046 MD 962449-1 -0.02649 0.00259 0.02908 ABS Diff. 09/20/96 1312 PDS 962449-1 960917G 2.14411 2.0000 0.00259 107.1 X REC 09/20/96 1322 CCV 9606107 5.04086 5.0 100.8 X REC 09/20/96 1343 CLB 9608022 -0.01139 09/20/96 1412 MD 962556-1 0.11242 0.10957 0.00285 ABS Diff. 09/20/96 1451 PDS 962556-1 960917G 2.10379 2.0000 0.10957 99.7 Y. REC 09/20/96 1456 Page 22 ineammcai re[w~5 o0 ons or n~a~w~u~am v'on ianq in rnir~mon ar.pe.ee ~iqn nrm~~~~on ane mp ern wooi~s~gire a~ni w~wnur..cYw~am cm.awxm ..e rnn mm q~~nnrryea Nem~p nirn wia Wnon,n ~niem.i. iu^. uio nisi nerwni ine u.i i~opr.e i of ~or0 um~aio~~a Cen Veer, i~.~n ~oae~ ma.n ~o +er enry ~ rm~eu~u~~m e.o ev w ~mn~.n o M rl ~+ro e~o+ss~ n~x'iu n..vne •e ~o ~ e orm ain~ir vamp eonra~ma or ore ~~u tle~na o~