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i~J CORE LABORATORIES Q U A L I T Y C O N T R O L R E S U L T S Job Number: 962453 Date: 09/28/96 CUSTOMER: Greystone PROJECT: 484-03 ATTN: Ray Faciski Test Method........: EPA 200.7 Batch ............. : 13526 Analyst...: gag Method Description.: Metals Analysis(ICAP ), Trace Reporting Limit... : 0.001 Parameter..........: Beryllium (Be) Units ............. : mg/L OC Lab ID Reagent OC Result DC Result True Value Orig. Value Calc. Result Units Date/Time ICV 9606182 2.01798 2.00 100.9 % REC 09/20/96 0950 ICB 9608022 -0.00005 09/20(96 1024 ISB 960630H 0.51820 0.5000 103.6 X REC 09/20/96 1046 MD 962449-1 0.00081 0.00064 0.00017 ABS Diff. 09/20/96 1312 PDS 962449-1 960917G 1.99423 2.000 0.00064 99.7 X REC 09/20/96 1322 CCV 9606107 2.50641 2.5 100.3 X REC 09/20/96 1343 CCB 9608022 -0.00010 09/20/96 1412 MD 962556-1 0.00057 0.00062 0.00005 ABS Diff. 09!20!96 1451 PDS 962556-1 960917G 1.86317 2.000 0.00062 93.1 7. REC 09/20/96 1456 CCV 9606107 2.50936 2.5 100.4 Y. REC 09/20/96 1524 CCB 9608022 0.00020 09/20/96 1533 CCV 9606107 2.48765 2.5 99.5 X REC 09/20/96 1636 CCB 9608022 0.00009 09/20/96 1646 ISB 960630H 0.49221 0.5000 98.4 X REC 09/20/96 1658 CCV 9606107 2.50366 2.5 100.1 X REC 09/20/96 1705 CCB 9608022 0.00040 09/20/96 1715 Test Method........: EPA 200.7 Batch .............: 13526 Analyst...: gag Method Description.: Metals Anal ysis(ICAP), Trace Reporting Limit...: 0.0005 Parameter..........: Cadmium (Cd) Units .............: mg/L OC Lab ID Reagent DC Result OC Result True Value Orig. Value Calc. Result Units Date/Time ICV 9606182 1.98572 2.00 94.3 X REC 09!20!46 0450 ICB 9608022 0.00048 09/20/96 1024 ISB 960630H 1.09941 1.000 109.9 X REG 09/20/96 1046 MD 962449-1 0.18735 0.18681 0.3 RPD 09/20/96 1312 PDS 962449-1 960917G 1.20095 1.000 0.18681 101.4 X REC 09/20/96 1322 CCV 9606107 1.03504 1.0 103.5 y. REC 09/20/96 1343 CC8 4608022 -0.00020 09/20{96 1412 MD 962556-1 -0.00040 -0.00047 0.00007 ABS Diff. 09/20/96 1451 PDS 962556-1 960917G 0.98360 1.000 -0.00047 98.4 X REC 09/20/96 1456 CCV 9606107 1.04157 1.0 104.2 X REC 09/20/96 1524 CC8 9608022 -0.00021 09/20/96 1533 CCV 9606107 1.02736 1.0 102.7 X REC 09/20/96 1636 CCB 9608022 0.00030 09/20/96 1646 ISB 960630H 1.04722 1.000 104.7 X REC 09/20/96 1658 CCV 9606107 1.02715 1.0 102.7 X REC 09/20/96 1705 CCB 9608022 0.00001 09/20/96 1715 Test Method........: EPA 200.7 Batch ............ .: 13526 Analyst...: gag Method Description.: Metals Analysis(ICAP), Trace Reporting Limit.. .: 0.1 Parameter..........: Calcium (Ca) Units ............ .: mg/L OL Lab ID Reagent OL Result OC Result True Value Orig. Value Calc. Result Units Date/Time ICV 9604125 95.48641 100.000000 95.5 X REC 09/20/96 1003 ICB 9608022 -0.00003 09/20/96 1024 ISA 960323A 460.50726 500 92.1 X REC 09/20/96 1031 ISB 9606308 452.22781 500 90.4 X REC 09/20/96 1046 CCV 9606272 102.43688 100.00 102.4 X REC 09/20/96 1333 Page 21 ,.~~...~,.~.,.,,i,.,.~.>,iiwe .mm caa ~m,aa~., c".`.o .,o„~,~ ..,,..,o..,,,.~~,.~.~i.o.,.~...~~„Vwm.m~.~..ro..~,a,..a,..,~,,.~...,~o,.oo,,,~ar moo., oo..~so.a,~,m.,,,., o~