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B;,SELI:;E J'.EF,;_ Di.'J C'L:'+IC,1L-ItIIJCR,;L ;,IiALYSIS <br />ATTACfIMENT A <br /> I N F O R M A T I O N <br />' Required Plethods of Extraction & Analysis (b) <br />Core Location and Number on map and log X <br />Sam le Depth and Interval X <br />Geologic Formation X <br />Lithologic Classification e.g., sandstone X <br />Textural Analyses: Units <br />5, Sand ~: X Sieve Analysis; USDA, 1952; N1 <br />~ Silt X Hydrometer; USDA, 1952; N1 <br />$ Cla X Hydrometer; USDA, 1952; N1 <br />Total Combustible Solids X~a Dry Ash; D 317 -73; ASTM, 19 0; q2 <br />Total Noncombustible Solids E x (a Dr Ash; D 317 -73; ASTM, 19 0; N26 <br />Laboratory Chemistry: <br />Acidity <br />off-Paste X Saturated Paste; USDA, 19 9; N o <br />Iron - Total Fe ppm X AB-DTPA (~ or DTPA 2 <br />Manganese Mn p m X AB-DTPA (~ or DTPA 2 <br />Sulfur: ~ Ph rifle Sulfur ~ X D 2492-79•, ASTM, 1980; Part 26 <br />9o Sulfate Sulfur X D 2 92-79; ASTM, 19 0; Part 2 <br />o Organic Sulfur X D 2492-79; ASTM, 1980, Part 26 <br />$ Total Sulfur % X D 3177-75 ASTM, 19 0; Part 2 <br />valor ions l~allnliv-HlKallnltvl <br />Calcium ~Ca~ ppm X Saturated Paste Extract, USDA N 0 <br />Chloride Cl- ppm X Saturated Paste Extract, USDA N60 <br />Fluoride F- ppm X Saturated Paste Extract, USDA N60 <br />Magnesium Mg pm X Saturated Paste Extract, USDA /J 0 <br />Nitrogen: Nitrate NO - pm X Saturated Paste Extract, USDA N 0 <br />Phosphate PO - ppin X AB-DTPA 1 or Ammonium Bicarbonate 3 <br />Potassium Y, ppm X Saturated Paste Extract, USDA N60 <br />Sodium Na ppm X Saturated Paste Er,tract, USDA N 0 <br />Sulfate SO - p m X D~2-79; AST11, 19 0; Part 26 <br />Conductivity wnhos/cn X Saturated Paste Extract, USDA N 0 <br />Sodium Adsorption Ratio SAP, X Saturated Paste Extract, USDA N60 <br />Total Carbonate CO - ! X Acid Titration, 23~, USDA N 0 <br />toxic neavv petals <br />Arsenic As m X AB-DTPA <br />(~, or Ammonium Bicarbonate <br />Barium Ba p m _ <br />AB-pTPA 1 or DPTA 2 <br />Boron B ppm X Saturated Paste Extract, USDA N 0 <br />Cadmium Cd in X AB-DTPA 1 or DPTA 2 <br />Chromium Cr ppm _ AB-DTPA 1 or DPTA 2 <br />Copper Cu ppm X AB DTPA 1 or DPTA 2 <br />Lead Pb ppm X AB-DTPA 1 or DPTA 2 <br />Mercur Hg ppb X Acid Extract: U.S. EPA, 1979; 2 5.5 <br />Molybdenum Mo ppm X AB-DPTA 1 or Ammonium Oxilate 5 <br />tJickel tJi pm AB-DPTA 1 or DTPA 2 <br />Selenium Se ppm X AB-DPTA 1 or Ho[ 4later Extract 6 <br />Zinc Zn p m X AB-DTPA TI or DTPA 2 <br />oactfve <br />ross Al <br />ppm = mg/kg ppb = ug/kg (a) Carbonaceous Materials only <br />(b) See attached reference list <br />