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AGZ Laboratories, Inc. • • • • • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 w • • <br /> Ensero Solutions ACZ Project ID: L74595 <br /> i <br /> L74595-02 uVG547617 Arsenic,total M200.81CP-MS M1 Matrix spike recovery was high,the recoveryofthe <br /> associated control sample(LCS or LFB)was acceptable. <br /> WG547238 Cyanide,WAD SM4500-CN I,E-Colorimetric w/ Q6 Sample was received above recommended temperature. <br /> distillation <br /> SM4500-CN I,E-Colorimetrc w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG547743 Fluoride SM450OF-C Q6 Sample was received above recommended temperature. <br /> WG547434 Nitrate/Nitrite as N M353.2-H2SO4 preserved Q6 Sample was received above recommended temperature. <br /> M353.2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> W G547920 Phosphorus,total M365.1-Auto Ascorbic Acid Q6 Sample was received above recommended temperature <br /> (digest) <br /> M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL)- <br /> WG546810 Residue,Filterable(TDS)@180C SM2540C Q6 Sample was received above recommended temperature <br /> WG547083 Residue,Non-Filterable(TSS)@105C SM2540D HC Initial analysis within holding time.Reanalysis was past <br /> holding time,which was required due to a QC failure during <br /> the initial analysis <br /> SM2540D N1 See Case Narrative <br /> SM2540D Q6 Sample was received above recommended temperature. <br /> SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10z MDL). <br /> SM2540D Z3 Sample volume yielded a residue less than 2 5 mg <br /> WG547479 Sulfate D516-02/-07/-1 l- M3 The spike recovery value is unusable since the analyte <br /> TURBIDIMETRIC concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> D516-02/-07/-1 l- Q6 Sample was received above recommended temperature. <br /> TURBIDIMETRIC <br /> REPAD.15.06.05.01 <br /> L74595-2209021603 Page 15 of 25 <br />