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ACZ Laboratories, Inc. 0 • • • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 0 • • <br /> Ensero Solutions ACZ Project ID: L74595 <br /> AM <br /> L74595-01 ✓JG547617 Arsenic,total M200 8 ICP-MS M1 Matrix spike recovery was high,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable. <br /> WG547238 Cyanide,WAD SM4500-CN I,E-Colorimetric w/ Q6 Sample was received above recommended temperature. <br /> distillation <br /> SM4500-CN I,E-Colorimetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG547743 Fluoride SM450OF-C Q6 Sample was received above recommended temperature. <br /> WG547434 Nitrate/Nitrite as N M353.2-H2SO4 preserved Q6 Sample was received above recommended temperature. <br /> M353.2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG547920 Phosphorus,total M365.1-Auto Ascorbic Acid Q6 Sample was received above recommended temperature. <br /> (digest) <br /> M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDQ <br /> WG546810 Residue,Filterable(TDS)@180C SM2540C Q6 Sample was received above recommended temperature. <br /> WG547083 Residue,Non-Filterable(TSS)@105C SM2540D HC Initial analysis within holding time.Reanalysis was past <br /> holding time,which was required due to a QC failure during <br /> the initial analysis. <br /> SM2540D N1 See Case Narrative. <br /> SM2540D Q6 Sample was received above recommended temperature. <br /> SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> SM2540D Z3 Sample volume yielded a residue less than 2-5 mg <br /> WG547479 Sulfate D516-02/-07/-11- Q6 Sample was received above recommended temperature. <br /> TURBIDIMETRIC <br /> REPAD.15.06.05.01 <br /> L74595-2209021603 Page 14 of 25 <br />