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ACZ Laboratories, Inc. • • - • - • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 - • • <br /> Ouray Silver Mines ACZ Project ID: L71828 <br /> METHODPARAMETER QUAL DESCRIPTION <br /> L71828-04 ✓VG538856 Chloride SM4500CI-E RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG538066 Cyanide,total M335.4-Colorimetric w/ M2 Matrix spike recovery was low,the recovery of the <br /> distillation associated control sample(LCS or LFB)was acceptable. <br /> WG538959 Nitrate/Nitrite as N M353.2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG538176 Phosphorus,total M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG537858 Residue,Filterable(TDS)@180C SM2540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG537892 Residue,Non-Filterable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> SM2540D Z3 Sample volume yielded a residue less than 2.5 mg <br /> WG538421 Sulfate D516-02/-07/-11- M1 Matrix spike recovery was high,the recovery of the <br /> TURBIDIMETRIC associated control sample(LCS or LFB)was acceptable. <br /> L71828-05 VVG538292 Beryllium,dissolved M200.8 ICP-MS VC CCV recovery was above the acceptance limits.Target <br /> analyte was not detected in the sample[<MDL]. <br /> WG538856 Chloride SM4500CI-E RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG538292 Copper,dissolved M200.8 ICP-MS VC CCV recovery was above the acceptance limits.Target <br /> analyte was not detected in the sample[<MDL]. <br /> WG538066 Cyanide,total M335.4-Colorimetric w/ M2 Matrix spike recovery was low,the recovery of the <br /> distillation associated control sample(LCS or LFB)was acceptable. <br /> WG538959 Nitrate/Nitrite as N M353.2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG537858 Residue,Filterable(TDS)@180C SM2540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG537892 Residue,Non-Filterable(TSS)@105C SM2540D Z3 Sample volume yielded a residue less than 2.5 mg <br /> WG538378 Sodium,dissolved M200.7 ICP MA Recovery for either the spike or spike duplicate was outside <br /> of the acceptance limits;the RPD was within the <br /> acceptance limits. <br /> WG538421 Sulfate D516-02/-07/-1 l- M1 Matrix spike recovery was high,the recovery of the <br /> TURBIDIMETRIC associated control sample(LCS or LFB)was acceptable. <br /> REPAD.15.06.05.01 <br /> L71828-2203281 147 Page 22 of 26 <br />