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AUZ Laboratories, Inc. • , • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 • • <br /> Ouray Silver Mines ACZ Project ID: L69171 <br /> ACZ • WORKNUM •D ! • <br /> L69171-01 dVG532746 Acid Generation Potential(calc) M600/2-78-054 1.3 N1 See Case Narrative <br /> Acid Neutralization Potential(calc) M600/2-78-054 1 3 N1 See Case Narrative <br /> Acid-Base Potential(calc) M600/2-78-054 1 3 N1 See Case Narrative <br /> WG530787 Aluminum(1312) M6010D ICP RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG530915 Antimony(1312) M6020B ICP-MS M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> M6020B ICP-MS ZG The ICP or ICP-MS Serial Dilution was not used for data <br /> validation because the sample concentration was less than <br /> 50 times the MDL <br /> Arsenic(1312) M6020B ICP-MS ZH Serial Dilution exceeded the acceptance criteria Matrix <br /> interference[physical or chemical]is suspected <br /> Barium(1312) M6020B ICP-MS ZH Serial Dilution exceeded the acceptance criteria Matrix <br /> interference[physical or chemical]is suspected <br /> Beryllium(1312) M6020B ICP-MS RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG530612 Bicarbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> WG530712 Boron(1312) M6010D ICP RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG531493 Bromide(1312-DI) M300 0-Ion Chromatography HD Analysis is outside the intended scope of the method,which <br /> does not provide hold time information for soil extracts No <br /> hold time is observed for collection to extraction The <br /> referenced method hold time is observed for extraction4o- <br /> analysis <br /> M300.0-Ion Chromatography M2 Matrix spike recovery was low,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable <br /> M300 0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG530915 Cadmium(1312) M6020B ICP-MS RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG531038 Carbon,total organic(TOC)(1312-DI) SM5310B HD Analysis is outside the intended scope of the method,which <br /> does not provide hold time information for soil extracts No <br /> hold time is observed for collection to extraction The <br /> referenced method hold time is observed for extraction4o- <br /> analysis <br /> SM5310B Q6 Sample was received above recommended temperature <br /> SM5310B RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG530612 Carbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> WG531493 Chloride(1312-DI) M300 0-Ion Chromatography HD Analysis is outside the intended scope of the method,which <br /> does not provide hold time information for soil extracts No <br /> hold time is observed for collection to extraction The <br /> referenced method hold time is observed for extraction4o- <br /> analysis <br /> M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG530915 Chromium(1312) M6020B ICP-MS RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> Cobalt(1312) M6020B ICP-MS RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG530612 Conductivity @25C(1312-DI) SM2510B Q6 Sample was received above recommended temperature <br /> WG530915 Copper(1312) M6020B ICP-MS RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> REPAD.15.06.05.01 <br /> L691 71-21 1 2031 01 8 Page 19 of 25 <br />