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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs CO 80487 <br />(800) 334-5493 <br />o• <br />Ouray Silver Mines <br />ACZ Project ID L6y.9169 <br />:,t7.:'' <br />�: t�•T.�t <br />., . „ w� X`r[C•Y <br />WG530712 iron 1312) <br />M6010D ICP <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />val,dat�o i oecause the concentration of the duplicated <br />samD e ,s too low 'or accurate evaluation (< 1 Ox MDL) <br />WG530915 Lead ',1312l <br />M6020B ICP-MS <br />RD <br />For a sold matrix the duplicate RPD (spike or matrix) <br />exceeded the :,,ontro im t which s attributable to the non - <br />homogeneity of ine sample <br />M6020B ICP-MS <br />ZG <br />The ICP pr ICP-MS Serial Dilution was not used for data <br />val daton oeca ise the sample concent ation was less than <br />50 times the MDL <br />W G530787 Lim,um (1312) <br />M6010D ICP <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL) <br />Magnesium (1312) <br />M6010D ICP <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1Ox MDL) <br />WG530915 Manganese (1312) <br />M6020B ICP-MS <br />ZH <br />Serial Dilution exceeded the acceptance criteria Matrix <br />interference tphysical or chemical] is suspected <br />WG530581 Mercury (1312) <br />M7470A CVAA <br />Q6 <br />Sample was received above recommended temperature <br />M7470A CVAA <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1 Ox MDL) <br />WG530915 Molybdenum (1312) <br />M6020B ICP-MS <br />ZG <br />The ICP or ICP-MS Serial Dilution was not used for data <br />validation because the sample concentration was less than <br />50 times the MDL <br />Nickel (1312) <br />M60208 ICP-MS <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample ,s too low for accurate evaluation (< 1 Ox MDL) <br />WG530636 Nitrate/Nitrite as N (1312-DI) <br />M353 2 - Automated Cadmium <br />HD <br />Analysis is outside the intended scope of the method, which <br />Reduction <br />does not provide hold time information for soil extracts No <br />hold time is observed for collection to extraction The <br />referenced method hold time is observed for extraction -to - <br />analysis <br />M353 2 - Automated Cadmium <br />06 <br />Sample was e--eived above recommended temperature <br />Reduction <br />M353 2 - Automated Cadmium <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />Reduction <br />validation Decause the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1 Ox MDL) <br />Nrtnte as N (1312-DI) <br />M353 2 - Automated Cadmium <br />HD <br />Analysis is outside the intended scope of the method, which <br />Reduction <br />does not Provide hold time information for soil extracts No <br />hold time is observed for collection to extraction The <br />referenced method hold time is observed for extraction -to - <br />analysis <br />M353 2 - Automated Cadm,um <br />06 <br />Sample was received above recommended temperature <br />Reduction <br />M353 2 - Automated Cadmium <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />Reduction <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL) <br />WG531648 Nitrogen, ammonia (1312-DI) <br />M350 1 Auto Sal,cylate w1gas <br />HD <br />Analysis is outside the intended scope of the method, which <br />diffusion <br />does not provide hold time information for sod extracts No <br />hold time is observed for collection to extraction The <br />referenced method hold time is observed for extraction -to - <br />analysis <br />M350 1 Auto Salicylate w/gas <br />Q6 <br />Sample was received above recommended temperature <br />diffusion <br />WG530634 Phosphorus, ortho dissolved (1312-DI) <br />lv1365 1 - Automated Ascorbic <br />HD <br />Analysis is outside the intended scope of the method which <br />does not provide hold time information for soil extracts No <br />hold time is observed for collection to extraction The <br />referenced method hold time is observed for extraction -to - <br />analysis <br />M365 1 - Automated Ascorbic <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation Pecause the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL) <br />W G531173 Phosphorus Tota: �' 312-DI) <br />M365 1 - Auto Ascorbic Acid <br />HD <br />Analysis is outside the intended scope of the method, which <br />(digest) <br />does not provide hold time information for soil extracts No <br />hold time is observed for collection to extraction The <br />referenced method hold time is observed for extraction -to - <br />analysis <br />REPAD 15 06 05 01 <br />L69169-21 11231041 Page 23 of 28 <br />