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ACZLiaboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Ouray Silver Mines ACZ Project ID. L69169 <br />WG530712 Iron �1.312) M601OD ICP <br />WG530915 Lead '1312) <br />WG530787 Lithwm (1312) <br />Magnesium t 1312) <br />WG530915 Manganese (1312) <br />WG530581 Mercury(1312) <br />WG530915 Molybdenum t1312) <br />Nickel (1312) <br />WG530636 Nitrate/Nitrite as N (1312-DI) <br />Nitrite as N (1312-DI) <br />WG531648 Nitrogen, ammonia (1312-DI) <br />M60206 ICP-MS <br />M60206 ICP-MS <br />M6010D ICP <br />M6010D ICP <br />M6020B ICP-MS <br />M7470A CVAA <br />M7470A CVAA <br />M6020B ICP-MS <br />M6020B ICP-MS <br />M353 2 - Automated Cadmium <br />Reduction <br />M353 2 - Automated Cadmium <br />Reduction <br />M353 2 - Automated Cadmium <br />Reduction <br />N1353 2 - Automated Cadmium <br />Reduction <br />M353 2 - Automated Cadmium <br />Reduction <br />M353 2 - Automated Cadmium <br />Reduction <br />M350 1 Auto Salicylate w/gas <br />diffusion <br />M350 1 Auto Salicylate w,gas <br />diffusion <br />RA Relative Percent Difference (RPD) was not used for data <br />validar.on because the concentration of the duplicated <br />samole is too low for accurate evaluation (< 1 Ox MDL) <br />RD For a solid matrix the duplicate RPD (spike or matrix) <br />exceeded the control emit, which is attributable to the nori- <br />homogenedy of the sample <br />ZG The ICP or ICP-MS Serial Dilution was not used for data <br />val dation because the sample concentration was less than <br />50 times t^e MDL <br />RA Relat,ve Percent Difference (RPD) was not used for data <br />validation 'because the concentration of the duplicated <br />sample s too low for accurate evaluation (< 10x MDL) <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL) <br />ZH Ser al Dilution exceeded the acceptance criteria Matrix <br />interference [physical or chemical] is suspected <br />06 Sample was received above recommended temperature <br />RA Relative Percent Difference (RPD) was not used for data <br />validat,on because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1ux MDL) <br />ZG The ICP or ICP-MS Serial Dilution was not used for data <br />validation because the sample concentration was less than <br />50 times the MDL <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1 Ox MDL) <br />HD Analysis is outside the intended scope of the method, which <br />does not provide hold time information for soil extracts No <br />hold time is observed for collection to extraction The <br />referenced method hold time is observed for extraction -to - <br />analysis <br />06 Sample was received above recommended temperature <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1 Ox MDL) <br />HD Analysis is outside the intended scope of the method which <br />does not provide hold time information for sod extracts No <br />hold time �s observed for collection to extraction The <br />referenced method hold time is observed for extraction -to - <br />analysis <br />06 Sample was received above recommended temperature <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />samole is too low for accurate evaluation (< 1 Ox MDL) <br />HD Analysis is outside the intended scope of the method, which <br />does not provide hold time information for sod extracts No <br />hold time is observed for collection to extraction The <br />referenced method hold time is observed for extraction -to - <br />analysis <br />06 Sample was received above recommended temperature <br />WG530634 Phosphorus, ortho dissolved (1312-DI) M365 1 - Automated Ascorbic <br />HD Analysis is outside the intended scope of the method, which <br />does not provide hold time information for soil extracts No <br />hold time is observed for collection to extraction The <br />referenced method hold time is observed for extraction -to - <br />analysis <br />M365 1 - Automated Ascorbic <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1 Ox MDL) <br />W G531173 Phosphorus, Total (1312-DI) N1365 1 - Auto Ascorbic Acid <br />HD Analysis is outside the intended scope of the method, which <br />(digest) <br />does not provide hold time information for soil extracts No <br />hold time is observed for collection to extraction The <br />referenced method hold time is observed for extraction -to - <br />analysis <br />REPAD 15 06 05 01 <br />L69169-21 11231041 Page 20 of 28 <br />