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AOZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Golder Associates ACZ Project ID: L44806 <br />- : 7" - _.= - u -- -- :.. - r . - = Wig- <br />•::.fi <br />Bicarbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />WG449740 <br />Calcium, dissolved <br />L44806-07 NG449751 <br />Bicarbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature <br />WG449740 <br />Calcium, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />M300.0 - Ion Chromatography <br />RA <br />concentration in the sample is disproportionate to the spike <br />Hydroxide as CaCO3 <br />SM2320B - Titration <br />Q6 <br />level. The recovery of the associated control sample (LCS <br />SM4500H+ B <br />Q6 <br />pH measured at <br />or LFB) was acceptable. <br />WG449751 <br />Carbonate as CaCO3 <br />SM23206 - Titration <br />Q6 <br />Sample was received above recommended temperature <br />WG450092 <br />Chloride <br />M300.0 - Ion Chromatography <br />Q6 <br />Sample was received above recommended temperature <br />Total Alkalinity <br />SM2320B - Titration <br />M300 0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />SM2320B - Titration <br />Q6 <br />WG449740 <br />Calcium, dissolved <br />validation because the concentration of the duplicated <br />M3 <br />WG449751 <br />Carbonate as CaCO3 <br />SM2320B - Titration <br />sample is too low for accurate evaluation (< 10x MDL) <br />WG449751 <br />Hydroxide as CaCO3 <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature. <br />pH <br />SM4500H+ B <br />Q6 <br />Sample was received above recommended temperature <br />M300.0 - Ion Chromatography <br />pH measured at <br />SM4500H+ B <br />Q6 <br />Sample was received above recommended temperature. <br />WG450540 <br />Residue, Filterable (TDS) @180C <br />SM2540C <br />C5 <br />Confirmatory analysis was past holding time. Original result <br />pH measured at <br />SM4500H+ B <br />Q6 <br />not confirmed. <br />Residue, Filterable (TDS) @180C <br />SM2540C <br />SM2540C <br />Q6 <br />Sample was received above recommended temperature. <br />WG450092 <br />Sulfate <br />M300 0 - Ion Chromatography <br />DC <br />Sample required dilution. Non -target analyte exceeded <br />Q6 <br />calibration range <br />M300 0 - Ion Chromatography <br />Q6 <br />Sample was received above recommended temperature. <br />WG449751 <br />Total Alkalinity <br />SM2320B - Titration <br />Q6 <br />Sample was received above recommended temperature <br />L44806-08 NG449751 <br />Bicarbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />WG449740 <br />Calcium, dissolved <br />M200 7 ICP <br />M3 <br />WG449751 <br />Carbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />WG450092 <br />Chloride <br />M300.0 - Ion Chromatography <br />06 <br />M300.0 - Ion Chromatography <br />RA <br />WG449751 <br />Hydroxide as CaCO3 <br />SM2320B - Titration <br />Q6 <br />pH <br />SM4500H+ B <br />Q6 <br />pH measured at <br />SM4500H+ B <br />Q6 <br />WG449286 <br />Residue, Filterable (TDS) @180C <br />SM2540C <br />06 <br />WG450092 <br />Sulfate <br />M300.0 - Ion Chromatography <br />Q6 <br />WG449751 <br />Total Alkalinity <br />SM2320B - Titration <br />Q6 <br />L44806-09 NG449751 <br />Bicarbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />WG449740 <br />Calcium, dissolved <br />M200 7 ICP <br />M3 <br />WG449751 <br />Carbonate as CaCO3 <br />SM2320B - Titration <br />Q6 <br />WG450092 <br />Chloride <br />M300.0 - Ion Chromatography <br />DC <br />M300.0 - Ion Chromatography <br />Q6 <br />M300.0 - Ion Chromatography <br />RA <br />WG449751 <br />Hydroxide as CaCO3 <br />SM2320B - Titration <br />Q6 <br />pH <br />SM4500H+ B <br />Q6 <br />pH measured at <br />SM4500H+ B <br />Q6 <br />WG449432 <br />Residue, Filterable (TDS) @180C <br />SM2540C <br />Q6 <br />WG450092 <br />Sulfate <br />M300 0 - Ion Chromatography <br />Q6 <br />WG449751 <br />Total Alkalinity <br />SM2320B - Titration <br />Q6 <br />REPAD.15.06.05.01 <br />Sample was received above recommended temperature. <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature <br />Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL). <br />Sample was received above recommended temperature <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />Sample was received above recommended temperature. <br />Sample required dilution. Non -target analyte exceeded <br />calibration range. <br />Sample was received above recommended temperature <br />Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1 O MDL). <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature. <br />Sample was received above recommended temperature. <br />L44806-1807031405 Page 20 of 24 <br />