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1S'gv; s4 YP Analytical Report 4 <br /> Client: Cotter Corp <br /> Analyte: Chloride <br /> Prep Date: 01/24/2018 <br /> Analysis Date: O1/24/2018 <br /> Approved Method Source: 40 CFR 136.3 <br /> Prep ID: SM 4500-C1--1997 <br /> Analytical Method ID: SM 4500-CI--1997 <br /> Instrument: Titrimetric <br /> Matrix: Aqueous(water,wastewater,groundwater) <br /> Sample volume used: 100 mL <br /> Analyst: SE <br /> Location ID SmOate SCG 4 Results Flags RL Units <br /> MINE REFILL O1/16/18 418035.A 32 2 mg/L <br /> Client: Cotter Corp <br /> Analyte: Sulfate,S042- <br /> Prep Date: 01/23/2018 <br /> Analysis Date: 01/23/2018 <br /> Approved Method Source: 40 CFR 136.3 <br /> Prep ID: ASTM D516-07 <br /> Analytical Method ID: ASTM D516-07 <br /> Instrument: Evo 160,UV/VIS <br /> Matrix: Aqueous(water,wastewater,groundwater) <br /> Sample volume used: 100 mL Dilution Factor: 100 <br /> Analyst: SE <br /> Location ID Smp Date SCG# Results Flags MDL RL Units <br /> MINE REFILL O1/16/18 418035.A 3,786 12.0 59.0 mg/L <br /> Qualifiers: <br /> E—Extrapolated value Value exceeds calibration range <br /> H—Analysis exceeded holding time <br /> !—Estimated value detected below the RL/MRL <br /> S—Spike recovery outside acceptance limits <br /> U—Analyte not detected <br /> X—See case narrative Confidential and Privileged 7-Feb-I8 <br />