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186;rmQrroup Analytical Report 3 <br /> Client: Cotter Corp <br /> Analyte: Bicarbonate(As HCO3) <br /> Prep Date: 01/20/2018 <br /> Analysis Date: 01/20/2018 <br /> Approved Method Source: 40 CFR 136.3 <br /> Prep ID: Std.Methods 2320 B. <br /> Analytical Method ID: Std.Methods 2320 B. <br /> Instrument: Titrimetric <br /> Matrix: Aqueous(water,wastewater,groundwater) <br /> Sample volume used: 100 mL <br /> Analyst: SE <br /> Location ID SmaDate SCG# Results Flags RL Units <br /> MINE REFILL O1/16/18 418035.A 2,359 10 mg/L <br /> Client: Cotter Corp <br /> Analyte: Alkalinity(total as CaCO3) <br /> Prep Date: 01/20/2018 <br /> Analysis Date: 01/20/2018 <br /> Approved Method Source: 40 CFR 136.3 <br /> Prep ID: Std.Methods 2320 B. <br /> Analytical Method ID: Std.Methods 2320 B. <br /> Instrument: Titrimetric <br /> Matrix: Aqueous(water,wastewater,groundwater) <br /> Sample volume used: 100 mL <br /> Analyst: SE <br /> Location ID SmnDate SCG# Results Flags RL Units <br /> MINE REFILL O1/16/18 418035.A 2,359 10 mg/L <br /> Qualifiers <br /> E—Extrapolated value.Value exceeds calibration range <br /> H—Analysis exceeded holding time <br /> J—Estimated value detected below the RUMRL <br /> S—Spike recovery outside acceptance limits <br /> U—Analyte not detected <br /> X—See case narrative Confidential and Privileged 7-Feb-18 <br />