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ACZ Laboratories, Inc. Inorganic Extended <br /> 2773 Downhill Dnve Steamboat Spnngs, CO 80487 (800)334-5493 Qualifier Report <br /> Golder Associates ACZ Project ID: L41229 <br /> ACZ ID WORKNUM PARAMETER METHOD QUAL DESCRIPTION <br /> L41229-01 JVG437911 Chloride M300 0-Ion Chromatography DC Sample required dilution Non-target analyte exceeded <br /> calibration range <br /> M300 0-Ion Chromatography H2 Initial analysis within holding time Reanalysis for the <br /> required dilution was past holding time <br /> M300 0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG436440 Residue,Filterable(TDS)@180C SM2540C RO The duplicate originally assigned to this sample was not <br /> used for precision assessment because residue density <br /> exceeded the method limits Another duplicate in the batch <br /> was used to assess precision Method required duplicate <br /> frequency was not met <br /> WG437911 Sulfate M300 0-Ion Chromatography H2 Initial analysis within holding time Reanalysis for the <br /> required dilution was past holding time <br /> WG436792 Total Alkalinity SM2320B-Titration RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> L41229-02 J1/G437911 Chloride M300 0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG436440 Residue,Filterable(TDS)@180C SM2540C RO The duplicate originally assigned to this sample was not <br /> used for precision assessment because residue density <br /> exceeded the method limits Another duplicate in the batch <br /> was used to assess precision Method required duplicate <br /> frequency was not met <br /> WG437911 Sulfate M300 0-Ion Chromatography DC Sample required dilution Non-target analyte exceeded <br /> calibration range <br /> L41229-03 AIG437911 Chloride M300 0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG436377 Residue,Filterable(TDS)@180C SM2540C RO The duplicate originally assigned to this sample was not <br /> used for precision assessment because residue density <br /> exceeded the method limits Another duplicate in the batch <br /> was used to assess precision Method required duplicate <br /> frequency was not met <br /> WG437911 Sulfate M300 0-Ion Chromatography DC Sample required dilution Non-target analyte exceeded <br /> calibration range <br /> WG436792 Total Alkalinity SM2320B-Titration RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> L41229-04 J1G437911 Chloride M300 0-Ion Chromatography H2 Initial analysis within holding time Reanalysis for the <br /> required dilution was past holding time <br /> M300 0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG436440 Residue,Filterable(TDS)@180C SM2540C RO The duplicate originally assigned to this sample was not <br /> used for precision assessment because residue density <br /> exceeded the method limits Another duplicate in the batch <br /> was used to assess precision Method required duplicate <br /> frequency was not met <br /> WG437911 Sulfate M300 0-Ion Chromatography DC Sample required dilution Non-target analyte exceeded <br /> calibration range <br /> M300 0-Ion Chromatography H2 Initial analysis within holding time Reanalysis for the <br /> required dilution was past holding time <br /> WG436792 Total Alkalinity SM2320B-Titration RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> REPAD 15 06 05.01 <br /> L41229-1712200847 Page 17 of 25 <br />