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ACZ Laboratories, Inc. • • <br /> ' 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 N - • • <br /> Golder Associates ACZ Project ID: L37566 <br /> • WMA METHOD • a s <br /> L37566-01 NG424199 Bicarbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> ' Carbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> WG425180 Chloride M300 0-Ion Chromatography DC Sample required dilution Non-target analyte exceeded <br /> calibration range <br /> M300 0-Ion Chromatography Q6 Sample was received above recommended temperature <br /> ' M300 0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG424199 Hydroxide as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> 1 pH SM4500H+B 06 Sample was received above recommended temperature <br /> pH measured at SM4500H+B Q6 Sample was received above recommended temperature <br /> WG424116 Residue,Filterable(TDS)@180C SM2540C Q6 Sample was received above recommended temperature <br /> WG4251110 Sulfate M300 0-Ion Chromatography Q6 Sample was received above recommended temperature <br /> WG424199 Total Alkalinity SM2320B-Titration Q6 Sample was received above recommended temperature <br /> L37566-02 ✓UG424199 Bicarbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> ' Carbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> WG425180 Chloride M300 0-Ion Chromatography Q6 Sample was received above recommended temperature <br /> M300 0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG424199 Hydroxide as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> pH SM4500H+B Q6 Sample was received above recommended temperature <br /> pH measured at SM4500H+B Q6 Sample was received above recommended temperature <br /> ' WG424116 Residue,Filterable(TDS)@180C SM2540C Q6 Sample was received above recommended temperature <br /> WG425180 Sulfate M300 0-Ion Chromatography DC Sample required dilution Non-target analyte exceeded <br /> calibration range <br /> M300 0-Ion Chromatography Q6 Sample was received above recommended temperature <br /> ' WG424199 Total Alkalinity SM2320B-Titration Q6 Sample was received above recommended temperature <br /> L37566-03 NG424199 Bicarbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> Carbonate as CaCC3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> WG425180 Chloride M300 0-Ion Chromatography Q6 Sample was received above recommended temperature <br /> M300 0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG424199 Hydroxide as CaCO3 SM2320B-Titration 06 Sample was received above recommended temperature <br /> pH SM4500H+B Q6 Sample was received above recommended temperature <br /> pH measured at SM4500H+B Q6 Sample was received above recommended temperature <br /> WG424116 Residue,Filterable(TDS)@180C SM2540C Q6 Sample was received above recommended temperature <br /> WG425180 Sulfate M300 0-Ion Chromatography DC Sample required dilution Non-target analyte exceeded <br /> calibration range <br /> M300 0-Ion Chromatography Q6 Sample was received above recommended temperature <br /> ' WG424199 Total Alkalinity SM2320B-Titration Q6 Sample was received above recommended temperature <br /> REPAD.15.06.05.01 <br /> ' L37566-1706221642 Page 15 of 23 <br />