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ACZ Laboratories, Inc. <br />2773 Downhffl Drive Steamboat Springs. CO 80487 (600) 334-5493 <br />Mid Continent Testing Labs, Inc <br />ACZ Project ID: L34283 <br />ACZ ID WORKNUM PARAMETER .. <br />L34283-01 WG414562 Carbon total (TC) ASA No.9 29-2.2.4 CombusWMR <br />06 Sample was received above recommended temperature. <br />ASA No.9 29-2.2.4 CombusWMR <br />RA Relative Percent Difference (RPD) was not used for data <br />validation bemuse the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL). <br />Carbon total organic (TOC) ASA No.9 29-2.2.4 Combustion/1111 <br />05 Sample was received above recommended temperature. <br />ASA No.9 29-2.2.4 CombusWMR <br />RA Relative Percent Difference (RPD) was not used for data <br />validation bemuse the concentration of the duplicated <br />sample Is too low for accurate evaluation (< 10x MDL). <br />WG414570 Neutralization Potential as CSC03 M60012-76.054 3.2.3 <br />RA Relative Percent Difference (RPD) was not used for data <br />validation bemuse the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL). <br />WG414410 Sulfur Organic Residual M60012-70-054 3.2.."00 <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample Is too low for accurate evaluation (< 10x MDL). <br />Sulfur Pyritic Sulfide M60012-70-054 3.2.4 -MOD <br />R1 RPD exceeded the method or laboratory acceptance lim it. <br />See Case Narrative. <br />Sul" Sulfate M60012-78054 3.2.4 -MOD <br />RA Relative Percent Difference (RPD) was not used for data <br />validation bemuse the concentration of the duplicated <br />sample Is too low for accurate evaluation (< 10x MDL). <br />L34253-02 WG414562 Carbon total (TC) ASA No.9 29-2.2.4 CombusWMR <br />06 Sample was received above recommended temperature. <br />ASA No.9 29-2.2.4 CombustiordIR <br />RA Relative Percent Difference (RPD) was not used for data <br />validation bemuse the concentration of the duplicated <br />sample Is too low for accurate evaluation (< lax MDL) <br />Carbon total organic (TOC) ASA No.9 29-2.2.4 CombusWMR <br />06 Sample was received above recommended temperature. <br />ASA No.9 29-2.2.4 CombuslionAR <br />RA Relative Percent Difference (RPD) was not used for data <br />validation bemuse the coneer4ration of the duplicated <br />sample is too law for accurate evaluation (< 10x MDL) <br />WG414570 Neutralisation Potential as CaCO3 M60012-78054 3.2.3 <br />RA Relative Percent Difference (RPD) was not used for data <br />validation bemuse the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL). <br />WG414410 Sulfur Organic Residual M60012-78054 3.2.4 -MOD <br />RA Relative Percent Difference (RPD) was not used for data <br />validation bemuse the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1 O MDL) <br />Sulfur Pyritic Sulfide 1060012-78.054 3.2.4 -MOD <br />R1 RPD exceeded the method or laboratory acceptance I;miL <br />See Case Narrative. <br />Sulfur Sulfate M60012-78054 3.2.4 -MOD <br />RA Relative Percent Difference (RPD) was not used for data <br />validation bemuse the concentration of the duplicated <br />sample is too low for accurate evaluation (< 10x MDL). <br />11.3421113-03 WG414662 Carbon. total (TC) ASA No.9 29-2.2.4 CombusWrVIR <br />06 Sample was received above recommended temperature. <br />ASA No.0 29-2.2.4 CombustbMR <br />RA Relative Percent Difference (RPD) was not used for date <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1ox MDL). <br />Carbon total organic (TOC) ASA No.9 29-2 2.4 CombustioMR <br />06 Sample was received above recommended temperature. <br />ASA No.9 29-2 2.4 CombustkwAR <br />RA Relative Percent Difference (RPD) was not used for date <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (c lox MDL). <br />WG414570 Neutralization Potential as CaCO3 M60012-76-054 3.2.3 <br />RA Relative Percent Difference (RPD) was not used for da'w <br />validation because the concentration of the duplicated <br />sample is too low for accurate evaluation (< 1ox MDL). <br />WG414410 Sulfur Organic Residual M60012-78-054 3.2.4 -MOD <br />RA Relative Percent Difference (RPD)was not used for data <br />validation because the concentration of the duplicated <br />sample is too law for accurate evaluation (< 10x MDL). <br />Sulfur Pyritic Sulfide M60012-78-054 3.2.4 -MOD <br />R1 RPD exceeded the method or laboratory acceptance limit. <br />See Case Narrative <br />Sulfur Sulfate M600/2-78-054 3.2.4 -MOD <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the concentration of the duplicated <br />sample is too tow for accurate evaluation (< 10x MDL) <br />REPAD.15,06.05.01 <br />L34283-1612131713 Page 10 of 15 <br />