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ACiZ Laboratories, Inc. <br />9774 r)nwnhill Drive Steamboat Snrinos. CO 80487 (800) 334-5493 <br />New Elk Coal Co., LLC ACZ Sample ID: <br />L34102-01 <br />Project ID: Date Sampled: <br />11/10/16 14:25 <br />Sample ID: PAW 2 Date Received: <br />11/11/16 <br />Sample Matrix: <br />Ground Water <br />Inorganic Prep <br />.. aIr. A - <br />Total Hot Plate M200.2 ICP 11/16/16 14:16 aeb <br />Digestion <br />Total Recoverable M20U lCP 11/17/16 11:00 gss <br />Digestion <br />Metals Analysis <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />L34102-1611220823 Page 2 of 9 <br />Calcium, dissolved <br />M200.7 ICP <br />1 <br />109 <br />mg/L <br />0.1 <br />0.5 <br />11/17/16 19:07 <br />aeb <br />Iron, dissolved <br />M200.7 ICP <br />1 <br />1.88 <br />mg/L <br />0.02 <br />0.05 <br />11/17/16 19:07 <br />aeb <br />Iron, total <br />M200.7 ICP <br />1 <br />87.10 <br />mg/L <br />0.02 <br />0.05 <br />11/17/16 14:06 <br />aeb <br />Iron, total recoverable <br />M200.7 ICP <br />1 <br />90.70 <br />mg/L <br />0.02 <br />0.05 <br />11/18/16 13:12 <br />gss <br />Magnesium, dissolved <br />M200.7 ICP <br />1 <br />20.4 <br />mg/L <br />0.2 <br />1 <br />11/17/16 19:07 <br />aeb <br />Manganese, dissolved <br />M200.7 ICP <br />1 <br />1.460 <br />mg/L <br />0.005 <br />0.03 <br />11/17/16 19:07 <br />aeb <br />Manganese, total <br />M200.7 ICP <br />1 <br />2.160 <br />mg/L <br />0.005 <br />0.03 <br />11/17/16 14:06 <br />aeb <br />Potassium, dissolved <br />M200.7 ICP <br />1 <br />3 <br />mg/L <br />0.2 <br />1 <br />11/17/16 19:07 <br />aeb <br />Sodium, dissolved <br />M200.7 ICP <br />1 <br />70.3 <br />mg/L <br />0.2 <br />1 <br />11/17/16 19:07 <br />aeb <br />Wet Chemistry <br />Alkalinity as CaCO3 <br />SM2320B - Titration <br />Bicarbonate as <br />1 <br />448 <br />mg/L <br />2 <br />20 <br />11/12/16 0:00 <br />emk <br />CaCO3 <br />Carbonate as CaCO3 <br />1 <br />U mg/L <br />2 <br />20 <br />11/12/16 0:00 <br />emk <br />Hydroxide as CaCO3 <br />1 <br />U mg/L <br />2 <br />20 <br />11/12/16 0:00 <br />emk <br />Total Alkalinity <br />1 <br />448 <br />* mg/L <br />2 <br />20 <br />11/12/16 0:00 <br />emk <br />Cation -Anion Balance <br />Calculation <br />Cation -Anion Balance <br />-4.3 <br />% <br />11/21/16 0:00 <br />calc <br />Sum of Anions <br />12 <br />meq/L <br />11/21/16 0:00 <br />calc <br />Sum of Cations <br />11 <br />meq/L <br />11/21/16 0:00 <br />calc <br />Chloride <br />SM4500CI-E <br />1 <br />26.4 <br />* mg/L <br />0.5 <br />2 <br />11118/1611:46 <br />bsu <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />356 <br />mg/L <br />0.2 <br />5 <br />11/21/16 0:00 <br />calc <br />(dissolved) <br />Lab Filtration (0.45um <br />SOPWC050 <br />1 <br />11/11/16 16:52 <br />emk <br />filter) <br />Lab Filtration (0.45um) <br />M200.7/200.8/3005A <br />1 <br />11/14/16 13:45 <br />gss <br />& Acidification <br />Residue, Filterable <br />SM2540C <br />1 <br />562 <br />mg/L <br />10 <br />20 <br />11/17/16 14:06 <br />abd <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />4 <br />436 <br />* mg/L <br />20 <br />80 <br />11/15/16 13:35 <br />sck <br />Filterable (TSS) <br />@105C <br />Sodium Adsorption <br />USGS -11738-78 <br />1.6 <br />11/21/16 0:00 <br />calc <br />Ratio in Water <br />Sulfate <br />D516-021-07 - Turbidimetric <br />5 <br />83.5 <br />mg/L <br />5 <br />25 <br />11/17/16 16:16 <br />bsu <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />L34102-1611220823 Page 2 of 9 <br />