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waAm Laboratories, Inc. <br />9771 r)nWnhill nriva Rtaamhnat Snrinos. CO 80487 (800) 334-5493 <br />New Elk Coal Co., LLC <br />Project ID: <br />Sample ID: PAW 1 <br />Inorganic Prep <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />L33969-01 <br />11/03/16 14:15 <br />11/04/16 <br />Ground Water <br />Total Hot Plate M200.2 ICP 11/08/16 11:45 aeb <br />Digestion <br />Total Recoverable M200.2 ICP 11/14/16 10:04 aeb <br />Digestion <br />Metals Analysis <br />REPIN.02.06.05.01 "Please refer to Qualifier Reports for details. <br />L33969-1611161609 Page 2 of 9 <br />Calcium, dissolvedy <br />M200.7 ICP <br />1 <br />27.2 <br />mg/L <br />0.1 <br />0.5 <br />11/10/16 16:42 <br />aeb <br />Iron, dissolved <br />M200.7 ICP <br />1 <br />0.48 <br />mg/L <br />0.02 <br />0.05 <br />11/10/16 12:22 <br />aeb <br />Iron, total <br />M200.7 ICP <br />1 <br />134 <br />mg/L <br />0.02 <br />0.05 <br />11/09/16 16:15 <br />aeb <br />Iron, total recoverable <br />M200.7 ICP <br />1 <br />137 <br />mg/L <br />0.02 <br />0.05 <br />11/15/16 12:29 <br />aeb <br />Magnesium, dissolved <br />M200.7 ICP <br />1 <br />8.9 <br />mg/L <br />0.2 <br />1 <br />11/10/16 12:22 <br />aeb <br />Manganese, dissolved <br />M200.7 ICP <br />1 <br />0.085 <br />mg/L <br />0.005 <br />0.03 <br />11/10/16 12:22 <br />aeb <br />Manganese, total <br />M200.7 ICP <br />1 <br />1.810 <br />mg/L <br />0.005 <br />0.03 <br />11/09/16 16:15 <br />aeb <br />Potassium, dissolved <br />M200.7 ICP <br />1 <br />1.4 <br />mg/L <br />0.2 <br />1 <br />11/10/16 12:22 <br />aeb <br />Sodium, dissolved <br />M200.71CP <br />1 <br />14.9 <br />mg/L <br />0.2 <br />1 <br />11/10/16 12:22 <br />aeb <br />Wet Chemistry <br />ms <br />i. • <br />R 1r <br />! <br />'P <br />!. <br />Alkalinity as CaCO3 <br />SM2320B-Titration <br />Bicarbonate as <br />1 <br />119 <br />mg/L <br />2 <br />20 <br />11/08/16 0:00 <br />sck <br />CaCO3 <br />Carbonate as CaCO3 <br />1 <br />U mg/L <br />2 <br />20 <br />11/08/16 0:00 <br />sck <br />Hydroxide as CaCO3 <br />1 <br />U mg/L <br />2 <br />20 <br />11/08/16 0:00 <br />sck <br />Total Alkalinity <br />1 <br />119 <br />mg1L <br />2 <br />20 <br />11/08/16 0:00 <br />sck <br />Cation -Anion Balance <br />Calculation <br />Cation -Anion Balance <br />0.0 <br />% <br />11/16/16 0:00 <br />Calc <br />Sum of Anions <br />2.8 <br />meq/L <br />11/16/16 0:00 <br />talc <br />Sum of Cations <br />2.8 <br />meq/L <br />11/16/16 0:00 <br />talc <br />Chloride <br />SM4500CI-E <br />1 <br />9.2 <br />mg/L <br />0.5 <br />2 <br />11/14/1614:37 <br />bsu <br />Hardness as CaCO3 <br />SM2340B-Calculation <br />105 <br />mg/L <br />0.2 <br />5 <br />11/16116 0:00 <br />talc <br />(dissolved) <br />Lab Filtration (0.45um <br />SOPWC050 <br />1 <br />11/05/16 14:41 <br />sck <br />filter) <br />Lab Filtration (0.45um) <br />M200.7/200.8/3005A <br />1 <br />11/08/16 14:00 <br />aeb <br />& Acidification <br />Residue, Filterable <br />SM2540C <br />2 <br />128 <br />mg/L <br />20 <br />40 <br />11/04/16 16:54 <br />sck <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />4 <br />420 <br />mg/L <br />20 <br />80 <br />11/07/16 17:11 <br />sck <br />Filterable (TSS) <br />@105C <br />Sodium Adsorption <br />USGS - I1738-78 <br />0.64 <br />11/16/16 0:00 <br />talc <br />Ratio in Water <br />Sulfate <br />D516 -o2/ -o7 -Turbidimetric <br />1 <br />6.5 <br />mg/L <br />1 <br />5 <br />11/16/1613:59 <br />bsu <br />REPIN.02.06.05.01 "Please refer to Qualifier Reports for details. <br />L33969-1611161609 Page 2 of 9 <br />