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A <br />Analysis Information <br />Quality Control Sample <br />Batch Report <br />Workorder: 1604403 <br />Limits: Historical/Performance Preparation: IH Metals QC, Bulk Prep Analysis: IH Metals QC <br />Basis: ALS Laboratory Group Batch: IIPX/18725 (HBN: 164268) Batch: IICP/11986 (HBN: 164326) <br />Prepared By: Brian S. Stites Analyzed By: Peter P. Steen <br />Laboratory Control Sample - Laboratory Control Sample Duplicate <br />LCS: 488532 <br />Analyzed: 02/16/2016 11:43 <br />Dilution: 1 <br />Units: ug/L <br />LCSD: 488533 <br />Analyzed: 02/16/2016 11:46 <br />Dilution: 1 <br />Units: ug/L <br />Analyte <br />Result <br />Target <br />% Rec <br />QC Limits <br />Result <br />% Rec <br />RPD <br />QC Limits <br />Cadmium <br />719 <br />667 <br />108 <br />83.0 <br />118.5 <br />710 <br />106 <br />1.29 <br />0.0 <br />20.0 <br />Cobalt <br />725 <br />667 <br />109 <br />87.9 <br />116.5 <br />718 <br />108 <br />1.02 <br />0.0 <br />20.0 <br />Chromium <br />7060 <br />6670 <br />106 <br />78.7 <br />119.3 <br />7040 <br />106 <br />0.245 <br />0.0 <br />20.0 <br />Copper <br />698 <br />667 <br />105 <br />76.4 <br />130.4 <br />691 <br />104 <br />0.989 <br />0.0 <br />20.0 <br />Iron <br />6940 <br />6670 <br />104 <br />71.1 <br />125.4 <br />6950 <br />104 <br />0.243 <br />0.0 <br />20.0 <br />Lithium <br />6930 <br />6670 <br />104 <br />80.0 <br />120.0 <br />6830 <br />102 <br />1.55 <br />0.0 <br />20.0 <br />Magnesium <br />6940 <br />6670 <br />104 <br />80.0 <br />126.7 <br />6920 <br />104 <br />0.309 <br />0.0 <br />20.0 <br />Manganese <br />6950 <br />6670 <br />104 <br />86.3 <br />112.9 <br />7060 <br />106 <br />1.65 <br />0.0 <br />20.0 <br />Molybdenum <br />727 <br />667 <br />109 <br />80.0 <br />120.0 <br />721 <br />108 <br />0.844 <br />0.0 <br />20.0 <br />Nickel <br />730 <br />667 <br />110 <br />86.0 <br />118.2 <br />722 <br />108 <br />1.19 <br />0.0 <br />20.0 <br />Lead <br />7220 <br />6670 <br />108 <br />80.0 <br />120.0 <br />7160 <br />107 <br />0.898 <br />0.0 <br />20.0 <br />Phosphorus <br />7260 <br />6670 <br />109 <br />62.8 <br />130.8 <br />7110 <br />107 <br />2.05 <br />0.0 <br />20.0 <br />Selenium <br />7280 <br />6670 <br />109 <br />58.2 <br />144.7 <br />7180 <br />108 <br />1.42 <br />0.0 <br />20.0 <br />Silver <br />7050 <br />6670 <br />106 <br />69.4 <br />128.7 <br />7160 <br />107 <br />1.59 <br />0.01 <br />40.0 <br />Sodium <br />6920 <br />6670 <br />104 <br />75.0 <br />150.0 <br />6850 <br />103 <br />0.944 <br />0.0 <br />50.0 <br />Tellurium <br />7390 <br />6670 <br />111 <br />80.0 <br />120.0 <br />7270 <br />109 <br />1.58 <br />0.0 <br />20.0 <br />Thallium <br />7230 <br />6670 <br />108 <br />56.1 <br />143.6 <br />7130 <br />107 <br />1.35 <br />0.0 <br />20.0 <br />Titanium <br />686 <br />667 <br />103 <br />80.0 <br />120.0 <br />682 <br />102 <br />0.521 <br />0.0 <br />20.0 <br />Vanadium <br />6980 <br />6670 <br />105 <br />85.8 <br />120.1 <br />6960 <br />104 <br />0.323 <br />0.0 <br />20.0 <br />Yttrium <br />698 <br />667 <br />105 <br />80.0 <br />120.0 <br />711 <br />107 <br />1.75 <br />0.0 <br />20.0 <br />Zinc <br />7390 <br />6670 <br />111 <br />50.9 <br />171.3 <br />7400 <br />111 <br />0.126 <br />0.0 <br />20.0 <br />Zirconium <br />6740 <br />6670 <br />101 <br />80.0 <br />120.0 <br />6850 <br />103 <br />1.68 <br />0.0 <br />20.0 <br />QC Report Authorization (/S/ is an electronic signature that complies with 21 CFR Part 11) <br />Analyst Peer Review <br />/S/ Peter P. Steen /S/ Lauren Jones <br />02/16/2016 14:43 02/16/2016 16:35 <br />Symbols and Definitions <br />* - Analyte above reporting limit or outside of control limits <br />A - Sample result is greater than 4 times the spike added <br />• - Sample and Matrix Duplicate less than 5 times the reporting limit <br />• - Result is above the calibration range <br />RPD - Relative % Difference (Spike / Spike Duplicate) <br />ND - Not Detected (U - Qualifier also flags analyte as not detected) <br />NA - Not Applicable <br />QC results are not adjusted for moisture correction, where applicable <br />Page 3 of 3 Tuesday, February 16, 2016 QCS V4.1 <br />