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A <br />Analysis Information <br />Quality Control Sample <br />Batch Report <br />Workorder: 1604403 <br />Limits: Historical/Performance Preparation: IH Metals QC, Bulk Prep Analysis: IH Metals QC <br />Basis: ALS Laboratory Group Batch: IIPX/18725 (HBN: 164268) Batch: IICP/11986 (HBN: 164326) <br />Prepared By: Brian S. Stites Analyzed By: Peter P. Steen <br />Blank <br />LRB: 488531 <br />Analyzed: 02/16/2016 11:40 <br />Units: ug/L <br />Analyte <br />Result <br />MDL <br />RL <br />Aluminum <br />ND <br />100 <br />333 <br />Arsenic <br />ND <br />50 <br />167 <br />Beryllium <br />ND <br />0.25 <br />0.833 <br />Cadmium <br />ND <br />1.5 <br />5.00 <br />Calcium <br />ND <br />300 <br />1000 <br />Chromium <br />ND <br />33.3 <br />83.3 <br />Cobalt <br />ND <br />1.5 <br />5.00 <br />Copper <br />ND <br />10 <br />33.3 <br />Iron <br />ND <br />20 <br />333 <br />Lead <br />ND <br />12.5 <br />83.3 <br />Lithium <br />ND <br />10 <br />33.3 <br />Magnesium <br />ND <br />25 <br />83.3 <br />Manganese <br />ND <br />2.5 <br />8.33 <br />Molybdenum <br />ND <br />7.5 <br />25.0 <br />Nickel <br />ND <br />2.53 <br />8.33 <br />Phosphorus <br />ND <br />100 <br />333 <br />Platinum <br />ND <br />161 <br />537 <br />Selenium <br />ND <br />50 <br />167 <br />Silver <br />ND <br />5 <br />16.7 <br />Sodium <br />ND <br />75 <br />250 <br />Tellurium <br />ND <br />25 <br />83.3 <br />Thallium <br />ND <br />25 <br />83.3 <br />Titanium <br />ND <br />0.3 <br />5.00 <br />Vanadium <br />ND <br />1.5 <br />5.00 <br />Yttrium <br />ND <br />1.5 <br />5.00 <br />Zinc <br />ND <br />10 <br />33.3 <br />Zirconium <br />ND <br />10 <br />33.3 <br />Laboratory Control Sample - Laboratory Control Sample Duplicate <br />LCS: 488532 <br />Analyzed: 02/16/2016 11:43 <br />Dilution: 1 <br />Units: ug/L <br />LCSD: 488533 <br />Analyzed: 02/16/2016 11:46 <br />Dilution: 1 <br />Units: ug/L <br />Analyte <br />Result <br />Target <br />% Rec <br />QC Limits <br />Result % Rec <br />RPD <br />QC Limits <br />Aluminum <br />6760 <br />6670 <br />101 <br />81.0 <br />125.5 <br />6780 102 <br />0.307 <br />0.0 <br />20.0 <br />Arsenic <br />7040 <br />6670 <br />106 <br />86.2 <br />113.4 <br />6920 104 <br />1.60 <br />0.0 <br />20.0 <br />Beryllium <br />704 <br />667 <br />106 <br />83.8 <br />114.6 <br />716 107 <br />1.70 <br />0.0 <br />20.0 <br />Calcium <br />6900 <br />6670 <br />103 <br />72.5 <br />126.5 <br />6890 103 <br />0.151 <br />0.0 <br />20.0 <br />Page 2 of 3 Tuesday, February 16, 2016 QCS V4.1 <br />