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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Golder Associates <br />ACZ Project ID: L16930 <br />ACZ ID WORKNUM PARAMETER <br />METHOD <br />QUAL <br />DESCRIPTION <br />L16930 -01 WG359741 Barium, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG359985 Chloride <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non - target analyte exceeded <br />calibration range. <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />L16930 -02 WG359741 Barium, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG359985 Chloride <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />Sulfate <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non - target analyte exceeded <br />calibration range. <br />L16930 -03 WG359741 Barium, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG359985 Chloride <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />Sulfate <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non - target analyte exceeded <br />calibration range. <br />L16930 -04 WG359798 Copper, dissolved <br />M200.7 ICP <br />D1 <br />Sample required dilution due to matrix. <br />Manganese, dissolved <br />M200.7 ICP <br />D1 <br />Sample required dilution due to matrix. <br />Zinc, dissolved <br />M200.7 ICP <br />D1 <br />Sample required dilution due to matrix. <br />WG359985 Chloride <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG359968 Residue, Filterable (TDS) @180C <br />SM2540C <br />H2 <br />Initial analysis within holding time. Reanalysis for the <br />required dilution was past holding time. <br />WG359985 Sulfate <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non - target analyte exceeded <br />calibration range. <br />L16930 -05 WG359741 Barium, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />Sodium, dissolved <br />M200.7 ICP <br />BB <br />Target analyte detected in calibration blank at or above <br />acceptance limit. Sample value was > 10X the <br />concentration in the calibration blank. <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG359985 Chloride <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non - target analyte exceeded <br />calibration range. <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />REPAD.15.06.05.01 <br />L16930- 1403041518 Page 18 of 23 <br />