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2014-04-07_INSPECTION - M1985210
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2014-04-07_INSPECTION - M1985210
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Last modified
8/24/2016 5:41:55 PM
Creation date
4/15/2014 4:48:10 PM
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DRMS Permit Index
Permit No
M1985210
IBM Index Class Name
INSPECTION
Doc Date
4/7/2014
Doc Name
Soil Sampling & analytical results
From
Palmetto Environmental Group, LLC
To
DRMS
Email Name
MAC
Media Type
D
Archive
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(�Iacmnalyfical' <br />www.pacelabs.com <br />QUALITY CONTROL DATA <br />Project: Colorado Flagstone <br />Pace Project No.: 60165959 <br />Pace Analytical Services, Inc. <br />9608 Loiret Blvd. <br />Lenexa, KS 66219 <br />(913)599 -5665 <br />LABORATORY CONTROL SAMPLE: <br />1352550 <br />ND <br />.099 <br />.1 <br />0.075 <br />Spike LCS LCS <br />% Rec <br />Parameter <br />Units <br />Conc. Result % Rec <br />Limits Qualifiers <br />Xylene (Total) <br />mg /kg <br />.3 0.26 87 <br />79 -120 <br />1,2- Dichloroethane -d4 (S) <br />% <br />102 <br />75 -129 <br />4- Bromofluorobenzene (S) <br />% <br />100 <br />76 -123 <br />Toluene -d8 (S) <br />% <br />104 <br />80 -120 <br />MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1352551 <br />MS MSD <br />60165959001 Spike Spike <br />Parameter Units Result Conc. Conc. <br />1352552 <br />MS MSD MS MSD % Rec Max <br />Result Result % Rec % Rec Limits RPD RPD Qual <br />1,1,1,2 - Tetrachloroethane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.075 <br />0.077 <br />76 <br />77 <br />10 -151 <br />3 <br />44 <br />1,1,1 - Trichloroethane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.084 <br />0.085 <br />84 <br />85 <br />21 -144 <br />2 <br />43 <br />1,1,2,2 - Tetrachloroethane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.074 <br />0.076 <br />75 <br />76 <br />10 -151 <br />2 <br />46 <br />1,1,2 - Trichloroethane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.074 <br />0.079 <br />75 <br />79 <br />10 -140 <br />6 <br />46 <br />1,1- Dichloroethane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.080 <br />0.083 <br />81 <br />83 <br />19 -137 <br />4 <br />43 <br />1,1- Dichloroethene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.075 <br />0.078 <br />76 <br />78 <br />27 -143 <br />3 <br />41 <br />1,1- Dichloropropene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.081 <br />0.079 <br />81 <br />79 <br />19 -144 <br />2 <br />43 <br />1,2,3 -Trich to robe nzene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.055 <br />0.055 <br />55 <br />55 <br />10 -147 <br />0 <br />50 <br />1,2,3 - Trichloropropane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.074 <br />0.078 <br />75 <br />78 <br />10 -151 <br />4 <br />46 <br />1,2,4 - Trichlorobenzene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.055 <br />0.052 <br />55 <br />52 <br />10 -146 <br />6 <br />50 <br />1,2,4 - Trimethylbenzene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.059 <br />0.055 <br />60 <br />55 <br />10 -145 <br />7 <br />49 <br />1,2- Dibromo -3- chloropropane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.084 <br />0.084 <br />84 <br />84 <br />10 -152 <br />1 <br />48 <br />1,2- Dibromoethane (EDB) <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.080 <br />0.086 <br />81 <br />86 <br />13 -153 <br />7 <br />40 <br />1,2- Dichlorobenzene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.061 <br />0.060 <br />62 <br />60 <br />10 -147 <br />3 <br />48 <br />1,2- Dichloroethane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.084 <br />0.088 <br />85 <br />88 <br />21 -147 <br />5 <br />38 <br />1,2- Dichloroethene (Total) <br />mg /kg <br />ND <br />.2 <br />.2 <br />0.16 <br />0.17 <br />80 <br />83 <br />21 -139 <br />3 <br />44 <br />1,2- Dichloropropane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.088 <br />0.090 <br />89 <br />90 <br />15 -145 <br />2 <br />43 <br />1,3,5- Trimethylbenzene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.062 <br />0.056 <br />62 <br />56 <br />10 -144 <br />10 <br />48 <br />1,3- Dichlorobenzene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.059 <br />0.056 <br />59 <br />56 <br />10 -143 <br />6 <br />49 <br />1,3- Dichloropropane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.072 <br />0.077 <br />72 <br />77 <br />10 -135 <br />7 <br />42 <br />1,4- Dichlorobenzene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.057 <br />0.054 <br />57 <br />54 <br />10 -144 <br />5 <br />48 <br />2,2- Dichloropropane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.065 <br />0.067 <br />66 <br />67 <br />16 -137 <br />3 <br />44 <br />2- Butanone (MEK) <br />mg /kg <br />ND <br />.5 <br />.5 <br />0.48 <br />0.54 <br />97 <br />109 <br />10 -160 <br />12 <br />50 <br />2- Chlorotoluene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.061 <br />0.057 <br />61 <br />57 <br />10 -143 <br />7 <br />48 <br />2- Hexanone <br />mg /kg <br />ND <br />.5 <br />.5 <br />0.40 <br />0.47 <br />81 <br />95 <br />10 -160 <br />17 <br />50 <br />4- Chlorotoluene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.061 <br />0.056 <br />61 <br />56 <br />10 -144 <br />9 <br />47 <br />4- Methyl -2- pentanone (MIBK) <br />mg /kg <br />ND <br />.5 <br />.5 <br />0.44 <br />0.48 <br />88 <br />96 <br />10 -152 <br />9 <br />47 <br />Acetone <br />mg /kg <br />ND <br />.5 <br />.5 <br />0.50 <br />0.63 <br />100 <br />126 <br />10 -160 <br />23 <br />49 <br />Benzene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.080 <br />0.083 <br />80 <br />83 <br />22 -144 <br />4 <br />38 <br />Bromobenzene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.066 <br />0.068 <br />66 <br />68 <br />10 -150 <br />3 <br />46 <br />Bromochloromethane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.088 <br />0.091 <br />88 <br />91 <br />17 -142 <br />4 <br />45 <br />Bromodichloromethane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.082 <br />0.087 <br />83 <br />87 <br />10 -143 <br />5 <br />42 <br />Bromoform <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.075 <br />0.081 <br />75 <br />81 <br />10 -145 <br />8 <br />44 <br />Bromomethane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.061 <br />0.067 <br />61 <br />67 <br />10 -137 <br />10 <br />47 <br />Carbon disulfide <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.069 <br />0.072 <br />70 <br />72 <br />10 -142 <br />3 <br />44 <br />Carbon tetrachloride <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.085 <br />0.085 <br />86 <br />85 <br />15 -153 <br />0 <br />45 <br />Chlorobenzene <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.067 <br />0.068 <br />68 <br />68 <br />10 -145 <br />1 <br />46 <br />Chloroethane <br />mg /kg <br />ND <br />.099 <br />.1 <br />0.067 <br />0.070 <br />67 <br />70 <br />17 -134 <br />4 <br />42 <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not be reproduced, except in full, <br />Date: 04/03/2014 04:47 PM without the written consent of Pace Analytical Services, Inc.. Page 37 of 48 <br />
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