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Pace Analytical Services, Inc. <br />9608 (�Iacmnalyfica( Lenexa, , KS Blvd. <br />Lenexa, KS 66219 <br />www.pacelabs.com (913)599 -5665 <br />QUALITY CONTROL DATA <br />Project: Colorado Flagstone <br />Pace Project No.: 60165959 <br />LABORATORY CONTROL SAMPLE: <br />1352550 <br />Spike <br />LCS <br />LCS <br />% Rec <br />Parameter <br />Units <br />Conc. <br />Result <br />% Rec <br />Limits Qualifiers <br />1,2- Dichloropropane <br />mg /kg <br />.1 <br />0.10 <br />104 <br />80 -120 <br />1,3,5- Trimethylbenzene <br />mg /kg <br />.1 <br />0.085 <br />85 <br />78 -120 <br />1,3- Dichlorobenzene <br />mg /kg <br />.1 <br />0.090 <br />90 <br />80 -120 <br />1,3- Dichloropropane <br />mg /kg <br />.1 <br />0.090 <br />90 <br />75 -120 <br />1,4- Dichlorobenzene <br />mg /kg <br />.1 <br />0.089 <br />89 <br />80 -120 <br />2,2- Dichloropropane <br />mg /kg <br />.1 <br />0.078 <br />78 <br />65 -129 <br />2- Butanone (MEK) <br />mg /kg <br />.5 <br />0.51 <br />102 <br />55 -135 <br />2- Chlorotoluene <br />mg /kg <br />.1 <br />0.086 <br />86 <br />80 -120 <br />2- Hexanone <br />mg /kg <br />.5 <br />0.50 <br />100 <br />57 -136 <br />4- Chlorotoluene <br />mg /kg <br />.1 <br />0.088 <br />88 <br />77 -120 <br />4- Methyl -2- pentanone (MIBK) <br />mg /kg <br />.5 <br />0.54 <br />108 <br />71 -128 <br />Acetone <br />mg /kg <br />.5 <br />0.48 <br />96 <br />43 -144 <br />Benzene <br />mg /kg <br />.1 <br />0.096 <br />96 <br />80 -120 <br />Bromobenzene <br />mg /kg <br />.1 <br />0.098 <br />98 <br />80 -122 <br />Bromochloromethane <br />mg /kg <br />.1 <br />0.099 <br />99 <br />76 -122 <br />Bromodichloromethane <br />mg /kg <br />.1 <br />0.10 <br />101 <br />80 -120 <br />Bromoform <br />mg /kg <br />.1 <br />0.10 <br />101 <br />75 -124 <br />Bromomethane <br />mg /kg <br />.1 <br />0.081 <br />81 <br />38 -150 <br />Carbon disulfide <br />mg /kg <br />.1 <br />0.093 <br />93 <br />58 -137 <br />Carbon tetrachloride <br />mg /kg <br />.1 <br />0.094 <br />94 <br />75 -140 <br />Chlorobenzene <br />mg /kg <br />.1 <br />0.091 <br />91 <br />80 -120 <br />Chloroethane <br />mg /kg <br />.1 <br />0.086 <br />86 <br />65 -127 <br />Chloroform <br />mg /kg <br />.1 <br />0.094 <br />94 <br />74 -120 <br />Chloromethane <br />mg /kg <br />.1 <br />0.073 <br />73 <br />39 -138 <br />cis -1,2- Dichloroethene <br />mg /kg <br />.1 <br />0.099 <br />99 <br />76 -124 <br />cis -1,3- Dichloropropene <br />mg /kg <br />.1 <br />0.093 <br />93 <br />82 -120 <br />Dibromochloromethane <br />mg /kg <br />.1 <br />0.10 <br />101 <br />80 -124 <br />Dibromomethane <br />mg /kg <br />.1 <br />0.11 <br />107 <br />80 -120 <br />Dichlorodifluoromethane <br />mg /kg <br />.1 <br />0.066 <br />66 <br />16 -135 <br />Ethylbenzene <br />mg /kg <br />.1 <br />0.089 <br />89 <br />80 -120 <br />Hexachloro -1,3- butadiene <br />mg /kg <br />.1 <br />0.083 <br />83 <br />73 -138 <br />Isopropyl benzene (Cumene) <br />mg /kg <br />.1 <br />0.093 <br />93 <br />80 -136 <br />Methyl -tert-butyl ether <br />mg /kg <br />.1 <br />0.098 <br />98 <br />78 -121 <br />Methylene chloride <br />mg /kg <br />.1 <br />0.091 <br />91 <br />70 -123 <br />n- Butylbenzene <br />mg /kg <br />.1 <br />0.081 <br />81 <br />72 -132 <br />n- Propylbenzene <br />mg /kg <br />.1 <br />0.084 <br />84 <br />72 -127 <br />Naphthalene <br />mg /kg <br />.1 <br />0.10 <br />103 <br />77 -126 <br />p- Isopropyltoluene <br />mg /kg <br />.1 <br />0.088 <br />88 <br />78 -128 <br />sec - Butylbenzene <br />mg /kg <br />.1 <br />0.082 <br />82 <br />73 -134 <br />Styrene <br />mg /kg <br />.1 <br />0.093 <br />93 <br />79 -120 <br />tert- Butylbenzene <br />mg /kg <br />.1 <br />0.087 <br />87 <br />77 -130 <br />Tetrachloroethene <br />mglkg <br />.1 <br />0.085 <br />85 <br />78 -128 <br />Toluene <br />mg /kg <br />.1 <br />0.091 <br />91 <br />79 -120 <br />trans- l,2- Dichloroethene <br />mg /kg <br />.1 <br />0.091 <br />91 <br />76 -124 <br />trans- 1,3- Dichloropropene <br />mg /kg <br />.1 <br />0.099 <br />99 <br />80 -124 <br />Trichloroethene <br />mg /kg <br />.1 <br />0.092 <br />92 <br />80 -120 <br />Trichlorofluoromethane <br />mg /kg <br />.1 <br />0.084 <br />84 <br />64 -126 <br />Vinyl chloride <br />mg /kg <br />.1 <br />0.081 <br />81 <br />57 -132 <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not <br />be reproduced, <br />except in full, <br />Date: 04/03/2014 04:47 PM <br />without the written consent <br />of Pace Analytical Services, Inc.. <br />Page 36 of 48 <br />