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- www.wwzlab.com r Helena, W$77-472-0711 • Billings, W 800 - 735 -4489 • Casper, WY 888- 235 -0515 <br />Aae►�►esrF,ae'eeea° sabre. trrs� J Gillette, WY 866 -606 -7175 • Rapid City, SD 886 -672 -1225 • College Station, T% 888 - 690 -2218 <br />QA /QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: Cotter Corporation Report Date: 07/05/13 <br />Project: Schwartz GW 06/12/13 S27034 Work Order: C13060505 <br />Analyte Count Result Units RL ° /.REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.7 <br />480 <br />mg /L <br />460 <br />mg /L <br />176 <br />Analytical Run ICP4- C_130625A <br />Sample ID: ICV <br />7 Initial Calibration <br />Verification Standard <br />mg /L <br />0.00766 <br />06/25/13 11:52 <br />Aluminum <br />4.98 <br />mg /L <br />010 <br />100 <br />95 <br />105 <br />Calcium <br />50.0 <br />mg /L <br />0.50 <br />100 <br />95 <br />105 <br />Iron <br />5.01 <br />mg /L <br />0.030 <br />100 <br />95 <br />105 <br />Magnesium <br />49.8 <br />mg /L <br />0.50 <br />100 <br />95 <br />105 <br />Manganese <br />4.80 <br />mg /L <br />0.010 <br />96 <br />95 <br />105 <br />Potassium <br />48.8 <br />mg /L <br />0.50 <br />98 <br />95 <br />105 <br />Sodium <br />50.4 <br />mg /L <br />0.50 <br />101 <br />95 <br />105 <br />Sample ID: ICSA <br />Aluminum <br />Calcium <br />I ron <br />Magnesium <br />Manganese <br />Potassium <br />Sodium <br />Sample ID: ICSAB <br />Aluminum <br />Calcium <br />Iron <br />Magnesium <br />Manganese <br />Potassium <br />Sodium <br />Method: E200.7 <br />Sample ID: MB- 130625A <br />Aluminum <br />Calcium <br />I ron <br />Magnesium <br />Manganese <br />Potassium <br />Sodium <br />Sample ID: LFB- 130625A <br />Aluminum <br />Calcium <br />I ron <br />Magnesium <br />Manganese <br />Potassium <br />Sodium <br />7 Interference Check Sample A <br />480 <br />mg /L <br />460 <br />mg /L <br />176 <br />mg /L <br />494 <br />mg /L <br />- 0.0185 <br />mg /L <br />0.00766 <br />mg /L <br />-0.431 <br />mg /L <br />7 Interference Check Sample AB <br />479 <br />mg /L <br />459 <br />mg /L <br />176 <br />mg /L <br />494 <br />mg /L <br />0.420 <br />mg /L <br />0.00200 <br />mg /L <br />-0.366 <br />mg /L <br />0.10 <br />0.50 <br />0.030 <br />0.50 <br />0.010 <br />0.50 <br />0.50 <br />0.10 <br />0.50 <br />0.030 <br />0.50 <br />0.010 <br />0.50 <br />0.50 <br />96 <br />80 <br />120 <br />92 <br />80 <br />120 <br />88 <br />80 <br />120 <br />99 <br />80 <br />120 <br />96 <br />80 <br />120 <br />92 <br />80 <br />120 <br />88 <br />80 <br />120 <br />99 <br />80 <br />120 <br />84 <br />80 <br />120 <br />7 Method Blank <br />Run: ICP4- C_130625A <br />ND <br />mg /L <br />0.009 <br />ND <br />mg /L <br />0.02 <br />ND <br />mg /L <br />0.002 <br />0.06 <br />mg /L <br />0.01 <br />ND <br />mg /L <br />0.0010 <br />ND <br />mg /L <br />0.04 <br />ND <br />mg /L <br />0.2 <br />7 Laboratory Fortified Blank <br />Run: ICP4- C_130625A <br />0.947 <br />mg /L <br />0.10 <br />95 <br />85 115 <br />48.4 <br />mg /L <br />0.50 <br />97 <br />85 115 <br />0.930 <br />mg /L <br />0.030 <br />93 <br />85 115 <br />48.4 <br />mg /L <br />0.50 <br />97 <br />85 115 <br />0.903 <br />mg /L <br />0.010 <br />90 <br />85 115 <br />47.7 <br />mg /L <br />0.50 <br />95 <br />85 115 <br />48.5 <br />mg /L <br />0.50 <br />97 <br />85 115 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />ND - Not detected at the reporting limit. <br />06/25/13 12:07 <br />06/25/13 12:11 <br />Batch: R175216 <br />06/25/13 12:29 <br />06/25/13 12:33 <br />Page 8 of 21 <br />