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14 10 A • ~.energylab.com ! Helena, MT 877472 -0711 - Billings, MT 000- 735 -4489 - Casper, WY 888- 235 -0515 <br />11111111111aw go tEmal7maSkm 1152 Gillette, WY 866 -686 -7175 - Rapid City, SO 886- 672 -1225 - College Station, TX 888 - 690 -2218 <br />QA /QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: Cotter Corporation <br />Report Date: <br />07/12/13 <br />Schwartz GW 6/18/13 S27005 <br />Work Order: <br />C13060672 <br />rProject: <br />Analyte <br />Count Result <br />Units <br />RL <br />%REC <br />Low Limit <br />High Limit RPD <br />RPDLimit Qual <br />Method: <br />E200.8 <br />Analytical Run: ICPMS2- C_130626A <br />Sample ID: <br />ICV <br />5 Initial Calibration Verification Standard <br />06/26/13 17:00 <br />Antimony <br />0.0532 <br />mg /L <br />0.0010 <br />106 <br />90 <br />110 <br />Copper <br />0.0500 <br />mg /L <br />0.0010 <br />100 <br />90 <br />110 <br />Lead <br />0.0505 <br />mg /L <br />0.0010 <br />101 <br />90 <br />110 <br />Silver <br />0.0203 <br />mg /L <br />0.0010 <br />102 <br />90 <br />110 <br />Thallium <br />0.0516 <br />mg /L <br />0.0010 <br />103 <br />90 <br />110 <br />Method: <br />E200.8 <br />Batch: 37946 <br />Sample ID: <br />MB -37946 <br />5 Method Blank <br />Run: ICPMS2- C_130626A <br />06/26/13 19:41 <br />Antimony <br />0.0004 <br />mg /L <br />0.0001 <br />Copper <br />ND <br />mg /L <br />0.0002 <br />Lead <br />ND <br />mg /L <br />3E -05 <br />Silver <br />0.0007 <br />mg /L <br />8E -05 <br />Thallium <br />ND <br />mg /L <br />8E -05 <br />Sample ID: <br />LCS3 -37946 <br />5 Laboratory Control <br />Sample <br />Run: ICPMS2- C_130626A <br />06/26/13 19:44 <br />Antimony <br />0.551 <br />mg /L <br />00010 <br />110 <br />85 <br />115 <br />Copper <br />0.482 <br />mg /L <br />0.0050 <br />96 <br />85 <br />115 <br />Lead <br />0.507 <br />mg /L <br />0.0010 <br />101 <br />85 <br />115 <br />Silver <br />0.0499 <br />mg /L <br />0.0010 <br />98 <br />85 <br />115 <br />Thallium <br />0.475 <br />mg /L <br />0.00050 <br />95 <br />85 <br />115 <br />Sample ID: <br />C13050860- 005DMS3 <br />5 Sample Matrix Spike <br />Run: ICPMS2- C_130626A <br />06/26/13 20:09 <br />Antimony <br />0.550 <br />mg /L <br />0.0010 <br />110 <br />70 <br />130 <br />Copper <br />0.484 <br />mg /L <br />0.0050 <br />96 <br />70 <br />130 <br />Lead <br />0.518 <br />mg /L <br />0.0010 <br />103 <br />70 <br />130 <br />Silver <br />0.0509 <br />mg /L <br />0.0010 <br />102 <br />70 <br />130 <br />Thallium <br />0.488 <br />mg /L <br />000050 <br />98 <br />70 <br />130 <br />Sample ID: <br />C13050860- 005DMSD3 <br />5 Sample Matrix Spike Duplicate <br />Run: ICPMS2- C_130626A <br />06/26/13 20:12 <br />Antimony <br />0.536 <br />mg /L <br />0.0010 <br />107 <br />70 <br />130 2.5 <br />20 <br />Copper <br />0.474 <br />mg /L <br />0.0050 <br />94 <br />70 <br />130 2.2 <br />20 <br />Lead <br />0.499 <br />mg /L <br />0.0010 <br />100 <br />70 <br />130 3.6 <br />20 <br />Silver <br />0.0498 <br />mg /L <br />0.0010 <br />100 <br />70 <br />130 2.3 <br />20 <br />Thallium <br />0.473 <br />mg /L <br />0.00050 <br />95 <br />70 <br />130 3.0 <br />20 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />ND - Not detected at the reporting limit. <br />Page 11 of 22 <br />