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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Golder Associates ACZ Project ID: L12395 <br />REPAD.15.06.05.01 <br />Page 17 of 22 <br />L12395 -01 WG345301 Chloride <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG345122 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG345301 Sulfate <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />L12395 -02 WG345301 Chloride <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non - target analyte exceeded <br />calibration range. <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG345122 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG344918 pH <br />SM4500H+ B <br />ZW <br />Method deviation. The sample was centrifuged prior to <br />analysis due to high solid content. <br />WG345301 Sulfate <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG344918 Total Alkalinity <br />SM2320B - Titration <br />ZW <br />Method deviation. The sample was centrifuged prior to <br />analysis due to high solid content. <br />L12395 -03 WG345301 Chloride <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non - target analyte exceeded <br />calibration range. <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG345278 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG344805 Residue, Filterable (TDS) @180C <br />SM2540C <br />ZO <br />Concentration is based on a final residue greater than 200 <br />Mg. <br />WG345301 Sulfate <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />L12395 -04 WG345301 Chloride <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG345278 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG344805 Residue, Filterable (TDS) @180C <br />SM2540C <br />ZO <br />Concentration is based on a final residue greater than 200 <br />Mg, <br />WG345301 Sulfate <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non - target analyte exceeded <br />calibration range. <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />L12395 -05 WG345301 Chloride <br />M300.0 - Ion Chromatography <br />M1 <br />Matrix spike recovery was high, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />WG345278 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 O MDL). <br />WG344805 Residue, Filterable (TDS) @180C <br />SM2540C <br />ZO <br />Concentration is based on a final residue greater than 200 <br />Mg. <br />WG345301 Sulfate <br />M300.0 - Ion Chromatography <br />DC <br />Sample required dilution. Non - target analyte exceeded <br />calibration range. <br />M300.0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />REPAD.15.06.05.01 <br />Page 17 of 22 <br />