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www.dtergylab.com 0p' J Helena, W 077-472 -0711 • Billings, MT 800 - 735-4189 • Casper, WY 888 - 235 -6515 <br />Aft Im Gillette, WY 866 - 686 -7175 • Rapid City, SO 886- 672 -1225 0 College Station, TX 888- 690 -2218 <br />Sample ID: LFB- 130603A <br />Aluminum <br />Calcium <br />Iron <br />Magnesium <br />8 Laboratory Fortified Blank <br />0.941 <br />mg /L <br />47.3 <br />QA/QC Summary Report <br />0.949 <br />mg /L <br />47.5 <br />mg /L <br />85 115 <br />0.030 <br />Prepared by Casper, <br />WY <br />Branch <br />95 <br />85 115 <br />Revised Date: <br />06/18/13 <br />Client: Cotter <br />Corporation <br />Report Date: <br />06/13/13 <br />Project: Schwartz <br />5/16/13 S26979 <br />Work Order: <br />C13050681 <br />FAnalyte <br />Count Result Units <br />RL <br />%REC Low Limit <br />High Limit RPD <br />RPDLimit Qual <br />Method: <br />E200.7 <br />Analytical Run: ICP4- C_130603A <br />Sample ID: <br />ICV <br />8 <br />Initial Calibration Verification Standard <br />06/03/13 12:52 <br />Aluminum <br />4.98 mg /L <br />0.10 <br />100 <br />95 <br />105 <br />Calcium <br />50.0 mg /L <br />0.50 <br />100 <br />95 <br />105 <br />Iron <br />5.12 mg /L <br />0.030 <br />102 <br />95 <br />105 <br />Magnesium <br />50.0 mg /L <br />0.50 <br />100 <br />95 <br />105 <br />Manganese <br />4.88 mg /L <br />0.010 <br />98 <br />95 <br />105 <br />Potassium <br />50.2 mg /L <br />0.50 <br />100 <br />95 <br />105 <br />Sodium <br />51.0 mg /L <br />0.50 <br />102 <br />95 <br />105 <br />Zinc <br />0.996 mg /L <br />0.010 <br />100 <br />95 <br />105 <br />Sample ID: <br />ICSA <br />8 <br />Interference Check Sample A <br />06/03/13 13:06 <br />Aluminum <br />478 mg /L <br />0.10 <br />96 <br />80 <br />120 <br />Calcium <br />451 mg /L <br />0.50 <br />90 <br />80 <br />120 <br />Iron <br />177 mg /L <br />0.030 <br />89 <br />80 <br />120 <br />Magnesium <br />492 mg /L <br />0.50 <br />98 <br />80 <br />120 <br />Manganese <br />0.00675 mg /L <br />0.010 <br />Potassium <br />0.00723 mg /L <br />0.50 <br />Sodium <br />0.0208 mg /L <br />0.50 <br />Zinc <br />0.0193 mg /L <br />0.010 <br />Sample ID: <br />ICSAB <br />8 <br />Interference Check Sample AB <br />06/03/13 13:10 <br />Aluminum <br />477 mg /L <br />0.10 <br />95 <br />80 <br />120 <br />Calcium <br />452 mg /L <br />0.50 <br />90 <br />80 <br />120 <br />Iron <br />177 mg /L <br />0.030 <br />88 <br />80 <br />120 <br />Magnesium <br />494 mg /L <br />0.50 <br />99 <br />80 <br />120 <br />Manganese <br />0.452 mg /L <br />0.010 <br />90 <br />80 <br />120 <br />Potassium <br />0.00881 mg /L <br />0.50 <br />Sodium <br />-0.131 mg /L <br />0.50 <br />Zinc <br />0.857 mg /L <br />0.010 <br />86 <br />80 <br />120 <br />Method: <br />E200.7 <br />Batch: R174338 <br />Sample ID: <br />MB- 130603A <br />8 <br />Method Blank <br />Run: ICP4 -C 130603A <br />06/03/13 13:29 <br />Aluminum <br />ND mg /L <br />0.009 <br />Calcium <br />ND mg /L <br />0.02 <br />Iron <br />ND mg /L <br />0.002 <br />Magnesium <br />ND mg /L <br />0.01 <br />Manganese <br />ND mg /L <br />0.0010 <br />Potassium <br />ND mg /L <br />0.04 <br />Sodium <br />ND mg /L <br />0.2 <br />Zinc <br />0.003 mg /L <br />0.001 <br />Sample ID: LFB- 130603A <br />Aluminum <br />Calcium <br />Iron <br />Magnesium <br />8 Laboratory Fortified Blank <br />0.941 <br />mg /L <br />47.3 <br />mg /L <br />0.949 <br />mg /L <br />47.5 <br />mg /L <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />ND - Not detected at the reporting limit <br />06/03/13 13:32 <br />Page 10 of 25 <br />Run: ICP4- C_130603A <br />0.10 <br />94 <br />85 115 <br />0.50 <br />95 <br />85 115 <br />0.030 <br />95 <br />85 115 <br />0.50 <br />95 <br />85 115 <br />ND - Not detected at the reporting limit <br />06/03/13 13:32 <br />Page 10 of 25 <br />