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Aral Laboratories, Inc. <br />2773 Downhill Drive Steamboat Spnngs, CO 80487 (800) 334-5493 <br />Seneca Coal Company <br />ACZ Sample ID: <br />L11835-05 <br />Project ID: 451129821 <br />Date Sampled. <br />04130113 09:10 <br />Sample ID: NPDES16 <br />Date Received: <br />04130113 <br />Sample Matrix: <br />Surface Water <br />Inorganic Prep <br />Acidify and filter Colorado 5 CCR 1002-31.5.31 05/03/13 10 55 las <br />(Potentially Dissolved) (2009) <br />Total Recoverable M200.2 ICP-MS 05/03/13 18,15 las <br />Digestion <br />Total Recoverable M200.2 ICP 05/07/13 12 49 aeb <br />Digestion <br />Metals Analysis <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 8 of 24 <br />1 '4! <br />Calcium, dissolved <br />M200.7 ICP <br />68.1 <br />mg/L <br />0.2 <br />1 <br />05/03/13 14:15 <br />aeb <br />Iron, total recoverable <br />M200.7 ICP <br />—.3.61 <br />mg/L <br />0.02 <br />0.05 <br />05/07/13 17:14 <br />aeb <br />Magnesium, dissolved <br />M200.7 ICP <br />38.6 <br />mg/L <br />0.2 <br />1 <br />05/03/13 14:15 <br />aeb <br />Potassium, dissolved <br />M200.7 ICP <br />3.7 <br />mg/L <br />0.3 <br />2 <br />05/03/13 14:15 <br />aeb <br />Selenium, dissolved <br />M200.8 ICP-MS <br />0.8 <br />ug/L <br />0.1 <br />03 <br />05/08/13 0.54 <br />msh <br />Selenium, potentially <br />M200.8 ICP-MS <br />1.2 <br />ug/L <br />0.1 <br />0.3 <br />05/07/13 2:43 <br />pmc <br />dissolved <br />Selenium, total <br />M200.8 ICP-MS <br />1.2 <br />ug/L <br />0.1 <br />0.3 <br />05/06/13 19:16 <br />msh <br />recoverable <br />Sodium, dissolved <br />M200.7 ICP <br />6.2 <br />mg/L <br />0.3 <br />2 <br />05/03/13 14 15 <br />aeb <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 8 of 24 <br />