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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Spnngs, CO 80487 (800) 334 -5493 <br />Seneca Coal Company <br />Project ID: 450855601 <br />Sample ID: NPDES8 <br />Inorganic Prep <br />ACZ Sample ID: <br />L12570 -01 <br />Date Sampled: <br />06110113 09:00 <br />Date Received: <br />06110113 <br />Sample Matrix: <br />Surface Water <br />Acidify and filter Colorado 5 CCR 1002- <br />06/12/13 15 23 <br />[as <br />(Potentially Dissolved) 31.5.31 (2009) <br />Total Hot Plate M200.2 ICP -MS <br />06/20/13 1900 <br />]as <br />Digestion <br />Total Recoverable M200.2 ICP -MS <br />06/11/13 12 59 <br />]as <br />Digestion <br />Total Recoverable M200.2 ICP <br />06/11/13 15:58 <br />scp <br />Digestion <br />Metals Analysis <br />�. i�o <br />.s��i <br />ix <br />e <br />b,'c,ca•„a,.^s:., w.. .tio°t"W- A>, -wG ?� , �i» xww% a.°„ L"' ���, ,. w"' ,.4y..;•,.:s....s��,r',»C� <br />>;. °. e�•YntK <br />.p"ei„{`,F,��i °_R:.� �;av:ik<b;..i <br />s z..w *��p .i�,.. <br />Iron, total recoverable M200.7 ICP 1 <br />0.27 <br />mg /L <br />0.02 <br />0.05 06/12/13 1602 <br />llc <br />Selenium, potentially M200.8 ICP -MS 1 <br />7.1 <br />ug /L <br />0.1 <br />03 06/13/13 2.20 <br />pmc <br />dissolved <br />Selenium, total M200.8 ICP -MS 2 <br />1.2 <br />ug /L <br />0.2 <br />0.5 06/21/13 23.21 <br />pmc <br />potentially dissolved <br />Selenium, total M200.8 ICP -MS 1 <br />1.4 <br />ug /L <br />0.1 <br />0.3 06/12/13 1 58 <br />pmc <br />recoverable <br />Wet Chemistry <br />i' ,.} a lam" :a r' -6 A: � }'�v9�§'a, fi, ;_yt -•qT °. <br />n -• ne'f+s.'„'.c >s` i��' - ��w,mss- «4k�'.o....A-L ;spg°' bsM,•i i,b'r .ids% T.. y ,2n Ax ^ •w r?m4 <br />., <br />ms's« X,¢b...,. ,. „s>r <br />'.;taY -,�� ..,;.. , <br />. , m, m, .a ,i.,,. ,,.- .x.,;�w�c' %a fib•_ .y;'9 »r <br />,.uY 1.5, FE ,as. <br />�, 6e s. '.,r,�"„ %'sia•� v ,';'�h '„ <br />> ,, ., s <br />Lab Filtration (glass SOPWC050 1 <br />06/11/13 11:39 <br />jad <br />fiber filter) <br />Residue, Filterable SM2540C 1 <br />2740 <br />mg /L <br />10 <br />20 06/11/13 10:21 <br />dew <br />(TDS) @180C <br />REPIN.02.06.05.01 ' Please refer to Qualifier Reports for details <br />Page 2 of 11 <br />