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J4LjL Laboratories, Inc. <br />2773 Downhill Drive Steamboat SOnnas. CO 80487 (800) 334 -5493 <br />City of Ouray <br />ACZ Sample ID: <br />L94059 -01 <br />Project ID: <br />L71055 <br />Date Sampled: <br />04110112 13:30 <br />Sample ID: <br />REVENUE 2012 <br />Date Received: <br />04113112 <br />1 <br />5 <br />Sample Matrix: <br />Soil <br />Vanadium (1312) <br />M6010B ICP <br />U * mg /L 0.005 0.03 04/27112 1315 aeb <br />Vanadium, total (3050) M6010B ICP <br />40.0 mg /Kg 0.5 3 <br />04127/12 14.34 aeb <br />Zinc (1312) <br />M6010B ICP <br />U * mg /L 0.01 0.05 04127/12 13.15 aeb <br />Zinc, total (3050) <br />M6010B ICP <br />1760 mg /Kg 1 5 <br />04/27112 14.34 aeb <br />Soil Analysis <br />Sod Preparation <br />e-l-L .. Anaiya- <br />Air Dry at 34 Degrees <br />USDA No. 1, 1972 <br />Date Analyst <br />bsu <br />Acid Generation <br />M60012 -78 -054 1.3 <br />14 <br />t CaCO3 /Kt <br />1 <br />5 <br />05108/12 1542 <br />calc <br />Potential (calc on <br />M3050B ICP -MS <br />04/26/12 13:06 <br />me <br />Digestion - Hot Plate <br />M3050B ICP <br />04/26/12 13:06 <br />me <br />Sulfur total) <br />USDA No. 60 (2) <br />04/24/12 14:00 <br />cra <br />Extraction <br />Acid Neutralization <br />M600/2 -78 -054 1.3 <br />105 <br />t CaCO3 /Kt <br />1 <br />5 <br />05/08/12 15.42 <br />calc <br />Potential (calc) <br />M1312 <br />04/24/12 20:40 <br />mss2 <br />Leaching Procedure <br />Acid -Base Potential <br />M600/2 -78 -054 1.3 <br />91 <br />t CaCO3 /Kt <br />1 <br />5 <br />05/08/12 1542 <br />calc <br />(calc on Sulfur total) <br />Neutralization <br />M600/2 -78 -054 3.2.3 <br />10.5 <br />* % <br />0.1 <br />0.5 <br />04/30/12 15:30 <br />ndj <br />Potential as CaCO3 <br />pH, Saturated Paste <br />USDA No. 60 (21A) <br />7.9 <br />units <br />0.1 <br />0.1 <br />04/25/12 11.30 <br />cra <br />Solids, Percent <br />CLPSOW390, PART F, D -98 <br />96.0 <br />% <br />0.1 <br />0.5 <br />04/16/12 16:07 <br />bsu <br />Sulfur Forms <br />M600/2 -78 -054 3.2.4 <br />Sulfur Organic <br />0.18 <br />% <br />0.01 <br />0.1 <br />04/27/12 0:00 <br />ndl <br />Residual <br />Sulfur Pyritic Sulfide <br />0.22 <br />* % <br />0.01 <br />0.1 <br />04/27/12 0:00 <br />nd) <br />Sulfur Sulfate <br />0.05 <br />B % <br />0.01 <br />0.1 <br />04/27/12 0:00 <br />ndl <br />Sulfur Total <br />0.45 <br />* % <br />0.01 <br />0.1 <br />04/27/12 0.00 <br />nd) <br />Total Sulfur minus <br />0.40 <br />% <br />0.01 <br />0.1 <br />04/27/12 0.00 <br />nd) <br />Sulfate <br />Sod Preparation <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 5 of 13 <br />e-l-L .. Anaiya- <br />Air Dry at 34 Degrees <br />USDA No. 1, 1972 <br />04/16/12 11:30 <br />bsu <br />C <br />Crush and Pulverize <br />EPA - 600/2 -78 -054 3.1.3 <br />04/26/12 10:45 <br />bsu <br />Digestion - Hot Plate <br />M3050B ICP -MS <br />04/26/12 13:06 <br />me <br />Digestion - Hot Plate <br />M3050B ICP <br />04/26/12 13:06 <br />me <br />Saturated Paste <br />USDA No. 60 (2) <br />04/24/12 14:00 <br />cra <br />Extraction <br />Sieve -250 um (60 <br />ASA No.9, 15 -4.2.2 <br />04/24/12 10:00 <br />me <br />mesh) <br />Synthetic Preap. <br />M1312 <br />04/24/12 20:40 <br />mss2 <br />Leaching Procedure <br />Synthetic Precip. <br />M1312, DI Water <br />04/25/12 22:40 <br />mss2 <br />Leaching Procedure <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 5 of 13 <br />