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AD Laboratories, Inc. <br />Seneca Coal Company ACZ Sample ID: L11653 -04 <br />Project 1D: 45/129821 Date Sampled: 04118113 11;30 <br />Sample ID: NPDES4 Date Received: 04118113 <br />Sample Matrix: Surface Water <br />Metals Analvsis <br />Iron, total recoverable <br />M200.7 ICP <br />0.21 <br />mg /L <br />0.02 <br />0.05 <br />04/23/13 12:17 <br />aeb <br />Selenium, potentially <br />M200.8 ICP -MS <br />4.9 <br />ug1L <br />0.1 <br />0.3 <br />04/19/13 23:32 <br />pmc <br />dissolved <br />Selenium, total <br />M200.8 ICP -MS <br />4.2 <br />ug/L <br />0.1 <br />0.3 <br />04/24/13 3:08 <br />pmc <br />recoverable <br />Wet Chemistry <br />Lab Filtration (glass <br />SOPWC050 <br />04/19/13 13:07 <br />dcw <br />fiber filter) <br />Residue, Filterable <br />SM2540C <br />3330 <br />mg /L <br />10 <br />20 <br />04/22/13 11:09 <br />dcw <br />(TDS) @180C <br />REPIN.02.06.05.01 <br />I <br />Page 6 of 14 <br />